Preparation method of fire prevention and extinguishing material for coal mine
A fire prevention and coal mine technology, applied in the field of flame retardant materials, can solve the problems of poor fire prevention effect and easy cracking, and achieve the effects of fire extinguishing, strong water retention and prevention of water loss
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[0039] Example 1
[0040] Take chitosan, ammonium persulfate, the mixed solution, the volume fraction of 1% acetic acid solution, mix the chitosan and the volume fraction of 1% acetic acid solution, and perform agitation to obtain reaction solution A, which is added to the reaction solution and mixed Liquid, constant temperature stirring treatment, that is reaction solution B, add ammonium persulfate to reaction solution B, continue to stir for 10 minutes, and then get the reactant; take the reactant, sodium-based montmorillonite, acrylic acid, water glass, N, N' -Methylene bisacrylamide, deionized water, mix the reactants and deionized water, and ultrasonically disperse to obtain a dispersion. Add acrylic acid, N,N'-methylene bisacrylamide, and sodium to the dispersion. The montmorillonite and water glass are stirred and reacted to obtain a semi-finished product; the semi-finished product is washed 3 times with deionized water, and the pH value is adjusted, and the precipitate i...
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[0041] Example 2
[0042] Take chitosan, ammonium persulfate, the mixed solution, the volume fraction of 1% acetic acid solution, mix the chitosan and the volume fraction of 1% acetic acid solution, and perform agitation to obtain reaction solution A, which is added to the reaction solution and mixed Liquid, constant temperature stirring treatment, to obtain reaction solution B, add ammonium persulfate to reaction solution B, continue to stir for 13 minutes, to obtain the reactant; take the reactant, sodium-based montmorillonite, acrylic acid, water glass, N, N' -Methylene bisacrylamide, deionized water, mix the reactants and deionized water, and ultrasonically disperse to obtain a dispersion. Add acrylic acid, N,N'-methylene bisacrylamide, and sodium to the dispersion. Montmorillonite and water glass are stirred and reacted to obtain a semi-finished product; wash the semi-finished product with deionized water 4 times, adjust the pH value, and filter to obtain a precipitate, wash...
Example Embodiment
[0043] Example 3
[0044] Take chitosan, ammonium persulfate, the mixed solution, the volume fraction of 1% acetic acid solution, mix the chitosan and the volume fraction of 1% acetic acid solution, and perform agitation to obtain reaction solution A, which is added to the reaction solution and mixed Liquid, constant temperature stirring treatment, namely reaction solution B, add ammonium persulfate to reaction solution B, continue to stir for 15 minutes, and then get the reactant; take the reactant, sodium-based montmorillonite, acrylic acid, water glass, N, N' -Methylene bisacrylamide, deionized water, mix the reactants and deionized water, and ultrasonically disperse to obtain a dispersion. Add acrylic acid, N,N'-methylene bisacrylamide, and sodium to the dispersion. The montmorillonite and water glass are stirred and reacted to obtain a semi-finished product; the semi-finished product is washed 5 times with deionized water, and the pH value is adjusted, and the precipitate is...
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