Device for circularly cleaning and dissolving chemicals and method for circularly cleaning and dissolving chemicals

A technology of chemicals and cleaning fluids, applied in chemical instruments and methods, cleaning methods and utensils, cleaning methods using liquids, etc., can solve problems affecting production efficiency, waste of water resources, and increase the difficulty of product debugging, etc., to achieve easy Effects of maintenance, saving resources, and accelerating dissolution rate

Active Publication Date: 2020-05-05
INST OF PROCESS ENG CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The above schemes all adopt the filtration and washing process for the ternary material reaction slurry, which causes a lot of waste of water resources and increases the difficulty of product debugging in the early stage
[0007] The raw material nickel cobalt manganese salt of the ternary material precursor needs a lot of time in the dissolution section. At present, stirring is usually used for dissolution, and the long time will affect the production efficiency.

Method used

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  • Device for circularly cleaning and dissolving chemicals and method for circularly cleaning and dissolving chemicals
  • Device for circularly cleaning and dissolving chemicals and method for circularly cleaning and dissolving chemicals
  • Device for circularly cleaning and dissolving chemicals and method for circularly cleaning and dissolving chemicals

Examples

Experimental program
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Effect test

Embodiment 1

[0064] This embodiment provides a device for circulating cleaning and dissolving chemicals, the schematic diagram of the device is as follows figure 1 shown. The device comprises: a sequentially connected chemical dissolution unit, a cleaning solution primary treatment unit, and a cleaning solution storage unit (i.e. figure 1 The cleaning water storage tank) and the cleaning liquid secondary treatment unit, the cleaning liquid secondary treatment unit is also connected with the chemical dissolution unit, and the chemical dissolution unit includes an ultrasonic dispersion tank.

[0065] The chemical dissolving unit includes three ultrasonic dispersing tanks: a nickel dissolving tank, a cobalt dissolving tank and a manganese dissolving tank. These three ultrasonic dispersing tanks are all connected to the cleaning liquid primary processing unit and the cleaning liquid secondary processing unit at the same time.

[0066] The cleaning liquid primary treatment unit includes a soli...

Embodiment 2

[0078] This embodiment provides a device for circulating cleaning and dissolving chemicals, except that the number of ultrasonic transducer vibrators placed on one side of the vibrating plate shell in the ultrasonic transducer vibrating plate is 14, and the number of vibrators between adjacent ultrasonic transducer vibrating elements is 14. Except that the spacing is 80mm, other aspects are the same as the device for circulating cleaning and dissolving chemicals provided in Example 1.

[0079] This embodiment also provides a method of using the device of this embodiment to perform circular cleaning and dissolve the raw material of the ternary material precursor, the specific method is:

[0080] (1) Pass the deionized water produced by the cleaning liquid secondary treatment unit into each tank in the device for circulating cleaning and dissolving chemicals, start the ultrasonic wave of the ultrasonic dispersion tank and start stirring, and clean the dirt in the tank , remove t...

Embodiment 3

[0087] This embodiment provides a device for circularly cleaning and dissolving chemicals, except that the number of ultrasonic transducer vibrators placed on one side of the vibrating plate shell in the ultrasonic transducer vibrating plate is 18, and the vibrators between adjacent ultrasonic transducer vibrating elements Except that the spacing is 60mm, other aspects are the same as the device for circulating cleaning and dissolving chemicals provided in Example 1.

[0088] This embodiment also provides a method of using the device of this embodiment to perform circular cleaning and dissolve the raw material of the ternary material precursor, the specific method is:

[0089] (1) Pass the deionized water produced by the cleaning liquid secondary treatment unit into each tank in the device for circulating cleaning and dissolving chemicals, start the ultrasonic wave of the ultrasonic dispersion tank and start stirring, and clean the dirt in the tank , remove the salt scale and ...

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Abstract

The invention provides a device for circularly cleaning and dissolving chemicals and a method for circularly cleaning and dissolving chemicals. The device comprises a chemicals dissolving unit, a cleaning fluid primary processing unit, a cleaning fluid storage unit and a cleaning fluid secondary processing unit which are connected in sequence, the cleaning fluid secondary processing unit is further connected with the chemicals dissolving units, and the chemicals dissolving unit comprises an ultrasonic dispersing tank. The method comprises the steps that 1) cleaning fluid produced by the cleaning fluid secondary processing unit is introduced into tank bodies, and ultrasounds are started; 2) cleaning fluid in the tank bodies is introduced into the cleaning fluid primary processing unit and introduced into the cleaning fluid storage unit; 3), the cleaning fluid in the cleaning fluid storage unit is introduced into the cleaning fluid secondary processing unit to be processed and recycled;and 4) the chemicals is placed in the ultrasonic dispersing tank, ultrasounds are started for accelerating dissolving. By means of the method, pollutants can be effectively removed, recycling of waterresource is realized, meanwhile, the dissolving speed of raw materials can be accelerated, and dispersing is homogenized.

Description

technical field [0001] The invention belongs to the field of chemical industry, and relates to a device for circulating cleaning and dissolving chemicals and a method for circulating cleaning and dissolving chemicals. Background technique [0002] Lithium-ion batteries have the advantages of high energy density, high working voltage, no memory response, small self-discharge, and long cycle life. They have been widely used in many fields such as mobile phones, notebook computers, pure electric vehicles, mobile base stations, and energy storage power stations. As the key material for the production of ternary cathodes for lithium-ion batteries, ternary precursors are mixed and sintered with lithium sources to form ternary cathodes, and their properties directly determine the core physical and chemical properties of ternary cathode materials. [0003] The synthesis method of the ternary material precursor is mainly the chemical co-precipitation method. Generally, the synthetic ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B08B3/12B08B13/00B01F11/02C02F9/04B01F1/00
CPCB08B3/12B08B13/00C02F9/00C02F1/001C02F1/283C02F1/42C02F2001/425C02F1/441B01F31/83
Inventor 谭强强冯海兰
Owner INST OF PROCESS ENG CHINESE ACAD OF SCI
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