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AE multi-element aerogel rubber-plastic blended closed-pore secondary mold pressing foaming material and preparation method thereof

A foaming material and secondary molding technology, applied in the field of polymer materials and their preparation, can solve the problems of uneven pore size, poor, poor dispersion, etc., and achieve the effect of avoiding uneven mixing and not easy to foam

Pending Publication Date: 2020-05-26
YIBAO FUJIAN POLYMER MATERIALS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the airgel of the present invention is added to this formula. After multiple attempts, the dispersion is seriously poor, the thermal conductivity fails to achieve a good result, and the uneven pore size is seriously poor.

Method used

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  • AE multi-element aerogel rubber-plastic blended closed-pore secondary mold pressing foaming material and preparation method thereof
  • AE multi-element aerogel rubber-plastic blended closed-pore secondary mold pressing foaming material and preparation method thereof
  • AE multi-element aerogel rubber-plastic blended closed-pore secondary mold pressing foaming material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0063] A preparation method of AE multi-component airgel rubber blended closed-cell secondary molding foaming material, comprising the following steps:

[0064] Food grade PVC premix:

[0065] According to the weight of the formula, first mix 100 parts of food grade PVC, 10 parts of heat insulation additive 409, 3 parts of structural stabilizer, 1 part of heat stabilizer, and 1 part of active agent for 18 minutes. The temperature reaches 80 After ℃, add 40 parts of processing aid (citric acid anhydrous food grade), continue to pressurize and stir until it reaches 135 ℃, and maintain it for 8 minutes;

[0066] When the rubber is mixed evenly and the temperature rises to 135°C, discharge the glue;

[0067] Open mill refining:

[0068] Put the sizing material obtained in the previous process into the open mill, and put the mixed material into the open mill, and knead for 8 minutes with a 2mm roller gap;

[0069] Calendering and standing:

[0070] The rubber material obtained ...

Embodiment 2

[0084] A preparation method of AE multi-component airgel rubber blended closed-cell secondary molding foaming material, comprising the following steps:

[0085] Food grade PVC premix:

[0086] According to the weight of the formula, 100 parts of food-grade PVC, 13 parts of heat insulation additive 409, 4 parts of structural stabilizer, 1.5 parts of heat stabilizer, and 1.5 parts of active agent are banburyed and blended for 20 minutes. The temperature reaches 80 After ℃, add 45 parts of processing aid (citric acid anhydrous food grade), continue to pressurize and stir until it reaches 140 ℃, and keep it for 10 minutes;

[0087] When the rubber is mixed evenly and the temperature rises to 140°C, remove the glue;

[0088] Open mill refining:

[0089] The sizing material obtained in the previous process is put into the open mill, and the mixed material is put into the open mill, and the 2mm roller gap is turned for 9 minutes;

[0090] Calendering and standing:

[0091] The ru...

Embodiment 3

[0105] A preparation method of AE multi-component airgel rubber blended closed-cell secondary molding foaming material, comprising the following steps:

[0106] Food grade PVC premix:

[0107] Mix 100 parts of food-grade PVC, 15 parts of thermal insulation additive 409, 5 parts of structural stabilizer, 2 parts of heat stabilizer, and 2 parts of active agent for 20 minutes and add 50 parts after the temperature reaches 80°C The processing aid (citric acid anhydrous food grade), continue pressurized stirring until reaching 140 ℃, maintain 10 minutes;

[0108] When the rubber is mixed evenly and the temperature rises to 140°C, remove the glue;

[0109] Open mill refining:

[0110] Put the sizing material obtained in the previous process into the open mill, put the mixed material into the open mill, and knead for 10 minutes with a 2mm roller gap;

[0111] Calendering and standing:

[0112] Put the sizing material obtained in the previous process into a 16-inch four-roller cal...

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Abstract

The invention discloses an AE multi-element aerogel rubber blended closed-pore secondary mold pressing foaming material. The material is prepared from the following components in parts by weight: 100parts of food-grade PVC, 20-30 parts of NBR, 40-50 parts of a processing aid, 10-15 parts of a heat-insulating aid, 3-5 parts of a structure stabilizer, 1-2 parts of a heat stabilizer, 1-2 parts of anactive agent, 0.5-1 part of a cross-linking agent, 10-15 parts of a foaming agent and 0.03-0.05 part of a color stabilizer. A proper formula and a proper process are combined, the formula componentsare creatively selected, the production technology breakthrough of high-dispersity, high-foaming-ratio, low-density, heat-preservation and heat-insulation products is effectively achieved, the densityis 70 + / -20 kg / m<3>, the heat conductivity coefficient is smaller than or equal to 0.020 W / m.k, and the material is small in heat conductivity and good in heat insulation performance.

Description

technical field [0001] The invention relates to the field of polymer materials and their preparation, in particular to AE multi-component airgel rubber-plastic blended closed-cell secondary molding foaming materials and a preparation method thereof. Background technique [0002] NBR and PVC are rubber blended mixed foam materials, among which NBR is the abbreviation of nitrile rubber, PVC is the abbreviation of polyvinyl chloride, and the blended rubber made of NBR and PVC is the main rubber used in combination with rubber and plastic at present. . The main advantages are heat preservation, good tensile strength, oil resistance, heat resistance and so on. [0003] In the prior art, when preparing NBR and PVC rubber blended mixed foam materials, processing aids are often added to increase fluidity. For example, application number CN201310395682.6 discloses light-colored NBR / PVC with high acrylonitrile content The preparation method of oil-resistant rubber material is mechan...

Claims

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Application Information

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IPC IPC(8): C08L27/06C08L9/02C08K13/02C08K5/092C08K3/22C08K5/09C08J9/10B29B7/00B29C44/34B29C44/04
CPCB29B7/002B29C44/04B29C44/3442C08J9/0023C08J9/0061C08J9/0066C08J9/0095C08J9/103C08J2203/04C08J2205/052C08J2327/06C08J2409/02
Inventor 侯汝红陈奕汲
Owner YIBAO FUJIAN POLYMER MATERIALS
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