One-step hydrothermal synthesis based on ionic liquid novel fluorescent carbon dots and detection application of one-step hydrothermal synthesis for sulfathiazole
A technology of fluorescent carbon dots and sulfathiazole, which is applied in the directions of fluorescence/phosphorescence, nano-carbon, luminescent materials, etc., can solve the problems of complex synthesis process of nano-fluorescent probes, low selectivity and sensitivity, and high synthesis cost, and achieve the detection rate. Fast, highly selective recognition performance, easy to operate effect
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Embodiment 1
[0020] Add 1.11 g of 1-allyl-3-vinylimidazolium tetrafluoroborate, 0.2602 g of malonic acid and 10 mL of pure water into a high-temperature reaction kettle, and conduct a hydrothermal reaction at 220 °C for 12 h. After separation and purification by a 0.22 μm filter membrane, it was diluted 50 times for use.
Embodiment 2
[0022] Add 1.11 g of 1-allyl-3-vinylimidazolium tetrafluoroborate, 0.5215 g of malonic acid and 10 mL of pure water into a high-temperature reaction kettle, and conduct a hydrothermal reaction at 180 °C for 12 h. After separation and purification by a 0.22 μm filter membrane, it was diluted 50 times for use.
Embodiment 3
[0024] Add 1.6650 g of 1-allyl-3-vinylimidazolium tetrafluoroborate, 0.7805 g of malonic acid and 10 mL of pure water into a high-temperature reaction kettle, and conduct a hydrothermal reaction at 220°C for 3 h. After separation and purification by a 0.22 μm filter membrane, it was diluted 50 times for use.
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