Flower fertilizer prepared from traditional Chinese medicine residues and used for Chrysalidocarpus lutescens and preparation method thereof
A manufacturing method and technology of traditional Chinese medicine dregs, applied in the direction of phosphate fertilizer, application, fertilization device, etc., can solve the problem of no control measures
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Embodiment 1
[0018] (1) Dry the dregs of traditional Chinese medicine, put them in a container, crush them through a 60-mesh sieve, and divide them into two parts on average, 100g each of dregs A and dregs B;
[0019] (2) 0.3g of tetrabutylammonium chloride was added into 100ml of water for dissolving, and the obtained solution was heated at a constant temperature at a temperature of 37°C, and then KH with a pH of 6.1 was added dropwise to the solution. 2 PO 4 / K 2 h 2 PO 4 Buffer solution, the dropping time is 60min until the system turns from clear to cloudy;
[0020] (3) adding the herb residue A crushed in step (1) into the mixing system of step (2), and using a microwave extractor to assist extraction for 45 minutes at a power of 100W, to obtain filtrate A;
[0021] (4) Extract the filtrate A for 5-10 min under the condition of microwave power of 600W and temperature of 95° C. to obtain filtrate B;
[0022] (5) The filtrate B is mixed with the dregs B in step (1), and then a mixt...
Embodiment 2
[0027] (1) Dry the dregs of traditional Chinese medicine, put them in a container, crush them through an 80-mesh sieve, and divide them into two parts on average, 100g each of dregs A and dregs B;
[0028] (2) 0.3g of tetrabutylammonium chloride was added into 100ml of water for dissolving, and the obtained solution was heated at a constant temperature at a temperature of 45°C, and then KH with a pH of 7.8 was added dropwise to the solution. 2 PO 4 / K 2 h 2 PO 4 Buffer solution, the dropping time is 60min until the system turns from clear to cloudy;
[0029] (3) Add a part of the medicinal residues pulverized in step (1) to the mixing system of step (2), and use a microwave extractor to assist extraction for 60 minutes at a power of 100W to obtain filtrate A;
[0030] (4) Extract the filtrate A for 5-10 min under the condition of microwave power of 600W and temperature of 95° C. to obtain filtrate B;
[0031] (5) The filtrate B is mixed with another portion of traditional...
Embodiment 3
[0036] (1) Dry the dregs of traditional Chinese medicine, put them in a container, crush them through a 70-mesh sieve, and divide them into two parts on average, 100g each of dregs A and dregs B;
[0037] (2) 0.3g of tetrabutylammonium chloride was added into 100ml of water for dissolving, and the obtained solution was heated at a constant temperature at a temperature of 35°C, and then KH with a pH of 6.7 was added dropwise to the solution. 2 PO 4 / K 2 h 2 PO 4 Buffer solution, the dropping time is 60min until the system turns from clear to cloudy;
[0038] (3) Add a portion of the medicinal residues pulverized in step (1) to the mixing system in step (2), and use a microwave extractor to assist extraction for 40-60min at a power of 100W to obtain filtrate A;
[0039] (4) Extract the filtrate A for 5-10 min under the condition of microwave power of 600W and temperature of 95° C. to obtain filtrate B;
[0040] (5) The filtrate B is mixed with another portion of traditional...
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