Temporary plugging workover fluid and preparation method thereof

A technology of workover fluid and expansion inhibitor, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., and can solve the problems of high water-absorbing resin expansion multiple, small temporary plugging layer pressure bearing capacity, and low temporary plugging success rate and other problems, to achieve the effects of easy degradation, improved pressure bearing capacity, and good pressure bearing capacity

Active Publication Date: 2022-06-03
PETROCHINA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The water-absorbing resin has a large water-absorbing expansion multiple, and its strength decreases after water-absorbing expansion. The pressure-bearing capacity of the temporary plugging layer is small, the adaptable range is small, and the success rate of temporary plugging is low.

Method used

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  • Temporary plugging workover fluid and preparation method thereof
  • Temporary plugging workover fluid and preparation method thereof
  • Temporary plugging workover fluid and preparation method thereof

Examples

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preparation example Construction

[0048] In the preparation process of the flour ball, the amount of water added can be 30% to 35% of the weight of the wheat flour, so that the flour and the floating beads can be mixed evenly and have plasticity.

[0049] In the preparation process of resin balls, the addition amount of isopropanol and silane coupling agent can be 20% to 25% and 2% to 3% of the weight of petroleum resin, respectively. As an interface modifier, it can make the petroleum resin and the floating ball more easily bonded together.

[0050] It should be noted that, in the embodiment of the present invention, the floating ball has a hollow structure, and the prepared flour ball and resin ball are also hollow, which makes the flour ball and the resin ball have lower densities.

[0051] The diameter of the polyvinyl alcohol fiber can be 0.01mm, 0.02mm, 0.03mm, etc., and the length can be 3mm, 4mm, 5mm, etc.

[0052] Wherein, the water absorption ratio of the resin ball in the embodiment of the present ...

Embodiment 1

[0083]The present embodiment provides a temporary plugging and workover fluid, which is prepared by the following method: adding 95.87 parts by weight of tap water into a stirring tank, and slowly adding 0.10 parts by weight of hydroxy sub-hydroxide to the stirring tank through an addition funnel under stirring state The aqueous solution of tetrasodium ethyldiphosphonate and pentasodium salt of aminotrimethylenephosphonate was stirred for 45min. Among them, the total mass percentage of hydroxyethylene diphosphonic acid tetrasodium salt and aminotrimethylenephosphonic acid pentasodium salt is 28%, hydroxyethylene diphosphonic acid tetrasodium salt and aminotrimethylenephosphonic acid pentasodium salt The mass ratio of 1:0.8. Under stirring conditions, add 0.29 parts by weight of a biopolymer with a molecular weight of 2 million to 6 million to the stirring tank, stir for 2.2 hours, and measure the dynamic shear force of the mixed liquid with a Marsh funnel for drilling fluid to...

Embodiment 2

[0087] The present embodiment provides a temporary plugging and workover fluid, which is prepared by the following method: adding 92.99 parts by weight of tap water into a stirring tank, and slowly adding 0.4 parts by weight of hydroxysulfite to the stirring tank through an addition funnel in a stirring state The aqueous solution of tetrasodium ethyl diphosphonic acid and pentasodium salt of aminotrimethylenephosphonic acid was stirred for 50 min. Among them, the total mass percentage of hydroxyethylene diphosphonic acid tetrasodium salt and amino trimethylene phosphonic acid pentasodium salt is 30%, hydroxyethylene diphosphonic acid tetrasodium salt and amino trimethylene phosphonic acid pentasodium salt The mass ratio is 1:1.2. Under stirring conditions, add 0.4 parts by weight of a biopolymer with a molecular weight of 2 million to 6 million into the stirring tank, stir for 2.5 hours, and measure the dynamic shear force of the mixed liquid with a Marsh funnel for drilling f...

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Abstract

The invention discloses a temporary plugging workover fluid and a preparation method thereof, belonging to the field of oil field chemistry. Based on 100 parts by weight, the temporary plugging workover fluid includes: 0.96-2.7 parts of flour balls, 0.48-1.35 parts of resin balls, 1.92-4.5 parts of swelling inhibitors, 0.29-0.45 parts of suspending agents, and 0.19-0.19 parts of fiber synergists 0.27 parts, 0.10-0.41 parts of antiscalant, 0.19-0.32 parts of degradation agent, and the balance is water; flour balls are mixed with wheat flour and floating beads with a mass ratio of 6:4-7:3, added water to mix, squeezed Made by pressing, cutting, forming and drying; the density of flour balls is 0.97‑1.02g / cm 3 , the particle size is 2‑4mm; resin balls are mixed with petroleum resin and floating beads with a mass ratio of 7:3‑8:3, then mixed with isopropanol and silane coupling agent, extruded, cut, shaped, and dried Prepared; the density of resin balls is 0.97‑1.02g / cm 3 , the particle size is 3-5mm; the fiber synergist is polyvinyl alcohol fiber; the diameter of polyvinyl alcohol fiber is 0.01-0.03mm, and the length is 3-5mm. The temporary plugging and workover fluid can form a temporary plugging layer with compact structure, excellent mechanical strength and pressure bearing capacity, and will not cause damage to the reservoir.

Description

technical field [0001] The invention relates to the field of oilfield chemistry, in particular to a temporary plugging workover fluid and a preparation method thereof. Background technique [0002] The leakage of workover fluid to the formation (referred to as lost circulation) not only affects the normal production of oil wells, but also pollutes the reservoir, causing loss of oil and gas production and economic losses to the oil field. The reasons for lost circulation include: high reservoir permeability, loose rock cementation, large pressure difference between reservoir and working fluid, etc. In the workover operation, the use of temporary plugging workover fluid can form a temporary plugging layer in the reservoir to prevent lost circulation. [0003] Currently used temporary plugging and workover fluids include superabsorbent resin and water, which can form stagnant gel clumps in the reservoir, accumulate in the reservoir, and block pore throats, thereby slowing lost...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/514
CPCC09K8/514C09K8/5083C09K2208/18
Inventor 樊松林杨晓春董军郭元庆王小芳尹瑞新赵俊峰辉建超李秀丽
Owner PETROCHINA CO LTD
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