Temporary plugging workover fluid and preparation method thereof
A technology of workover fluid and expansion inhibitor, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., and can solve the problems of high water-absorbing resin expansion multiple, small temporary plugging layer pressure bearing capacity, and low temporary plugging success rate and other problems, to achieve the effects of easy degradation, improved pressure bearing capacity, and good pressure bearing capacity
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[0048] In the preparation process of the flour ball, the amount of water added can be 30% to 35% of the weight of the wheat flour, so that the flour and the floating beads can be mixed evenly and have plasticity.
[0049] In the preparation process of resin balls, the addition amount of isopropanol and silane coupling agent can be 20% to 25% and 2% to 3% of the weight of petroleum resin, respectively. As an interface modifier, it can make the petroleum resin and the floating ball more easily bonded together.
[0050] It should be noted that, in the embodiment of the present invention, the floating ball has a hollow structure, and the prepared flour ball and resin ball are also hollow, which makes the flour ball and the resin ball have lower densities.
[0051] The diameter of the polyvinyl alcohol fiber can be 0.01mm, 0.02mm, 0.03mm, etc., and the length can be 3mm, 4mm, 5mm, etc.
[0052] Wherein, the water absorption ratio of the resin ball in the embodiment of the present ...
Embodiment 1
[0083]The present embodiment provides a temporary plugging and workover fluid, which is prepared by the following method: adding 95.87 parts by weight of tap water into a stirring tank, and slowly adding 0.10 parts by weight of hydroxy sub-hydroxide to the stirring tank through an addition funnel under stirring state The aqueous solution of tetrasodium ethyldiphosphonate and pentasodium salt of aminotrimethylenephosphonate was stirred for 45min. Among them, the total mass percentage of hydroxyethylene diphosphonic acid tetrasodium salt and aminotrimethylenephosphonic acid pentasodium salt is 28%, hydroxyethylene diphosphonic acid tetrasodium salt and aminotrimethylenephosphonic acid pentasodium salt The mass ratio of 1:0.8. Under stirring conditions, add 0.29 parts by weight of a biopolymer with a molecular weight of 2 million to 6 million to the stirring tank, stir for 2.2 hours, and measure the dynamic shear force of the mixed liquid with a Marsh funnel for drilling fluid to...
Embodiment 2
[0087] The present embodiment provides a temporary plugging and workover fluid, which is prepared by the following method: adding 92.99 parts by weight of tap water into a stirring tank, and slowly adding 0.4 parts by weight of hydroxysulfite to the stirring tank through an addition funnel in a stirring state The aqueous solution of tetrasodium ethyl diphosphonic acid and pentasodium salt of aminotrimethylenephosphonic acid was stirred for 50 min. Among them, the total mass percentage of hydroxyethylene diphosphonic acid tetrasodium salt and amino trimethylene phosphonic acid pentasodium salt is 30%, hydroxyethylene diphosphonic acid tetrasodium salt and amino trimethylene phosphonic acid pentasodium salt The mass ratio is 1:1.2. Under stirring conditions, add 0.4 parts by weight of a biopolymer with a molecular weight of 2 million to 6 million into the stirring tank, stir for 2.5 hours, and measure the dynamic shear force of the mixed liquid with a Marsh funnel for drilling f...
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