Silver metallic oxide electric contact material and preparation method thereof
A technology of oxide electricity and contact materials, which is applied in the direction of conductive materials dispersed in non-conductive inorganic materials, etc., can solve the problems of environmental pollution and high comprehensive cost, and achieve the goal of improving bonding strength, eliminating uneven distribution, and making the preparation process environmentally friendly. Effect
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Embodiment 1
[0038] a) 18kg silver is melted in the graphite crucible of intermediate frequency smelting furnace, forms silver melt;
[0039] b) 1.8 kg of SnO with an average particle size of 0.1 μm 2 powder and 0.2kg of WO with an average particle size of 1 μm 3 Mix the powder evenly, put it into the powder spraying device, and connect it with the upper spray plate of the high-pressure water atomization equipment; set the pressure of high-purity nitrogen in the powder spraying equipment to 0.2MPa, and the flow rate of the inert gas to 200L / min;
[0040] c) The lower spray plate of the high-pressure water atomization equipment is connected to high-pressure water, the water pressure is set to 20MPa, and the atomization equipment is turned on;
[0041] d) The molten silver is poured into the collection bucket from the center of the spray plate of the high-pressure water atomization equipment through the heat preservation crucible, and the powder spraying device is turned on, with high-purit...
Embodiment 2
[0045] a) 9kg of silver is melted in the graphite crucible of the intermediate frequency melting furnace to form silver melt;
[0046] b) Mix 0.9kg of CuO powder with an average particle size of 10μm, 0.05kg of NiO powder with an average particle size of 1μm, and 0.05kg of MgO powder with an average particle size of 12μm, put them into the powder spraying device, and connect them to the upper spray plate of the high-pressure water atomization equipment Pass; set the pressure of high-purity argon in the powder spraying equipment to 1.0MPa, and the flow rate of inert gas to 1000L / min;
[0047] c) The lower spray plate of the high-pressure water atomization equipment is connected to high-pressure water, the water pressure is set to 200MPa, and the atomization equipment is turned on;
[0048] d) The molten silver is poured into the collection bucket from the center of the spray plate of the high-pressure water atomization equipment through the heat preservation crucible, and the p...
Embodiment 3
[0052] a) 18.4kg silver is melted in the graphite crucible of intermediate frequency smelting furnace, forms silver melt;
[0053] b) 1.4 kg of ZnO powder with an average particle size of 2.5 μm and 0.1 kg of SnO with an average particle size of 2 μm 2 Powder, 0.1kg of La with an average particle size of 10μm 2 o 3 Mix the powder evenly, put it into the powder spraying device, and connect it to the upper spray plate of the high-pressure water atomization equipment; set the pressure of high-purity nitrogen in the powder spraying equipment to 0.5MPa, and the flow rate of the inert gas to 600L / min;
[0054] c) The lower spray plate of the high-pressure water atomization equipment is connected to high-pressure water, the water pressure is set to 100MPa, and the atomization equipment is turned on;
[0055] d) The molten silver is poured into the collection bucket from the center of the spray plate of the high-pressure water atomization equipment through the heat preservation cruc...
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