Production method of steel waste heat blackening agent

A technology of waste heat blackening and production method, which is applied in coatings, anti-corrosion coatings, polyether coatings, etc., can solve the problems of complex preparation methods and high cost, and achieve the effects of simple process, low cost and low energy consumption

Inactive Publication Date: 2020-08-21
镇江市乐嘉生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Aiming at the deficiencies in the prior art, the purpose of the present invention is to provide a production method of waste heat blackening agent for iron and

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Example 1: 12 parts of water mass fraction components, 2 parts of carbon black mass fraction components, 1 part of acetate-based resin mass fraction components, and 3 parts of wetting and dispersing agent mass fraction components are added to the reactor Among them, the stirring speed of water, carbon black, acetate resin and wetting and dispersing agent was 50r / min, the temperature was 20°C, and the stirring time was 5min to prepare mixture A;

[0030] Then the raw materials are mixed, the water-based pigment is added to the mixture A, and the stirring speed is controlled at 30r / min to disperse the water-based pigment into the mixture A to prepare the mixture B;

[0031] Next, add alkylphenol formaldehyde resin polyoxyethylene ether in mixture B, wherein the mass fraction component of alkylphenol formaldehyde resin polyoxyethylene ether is 25 parts, add alkylphenol formaldehyde resin polyoxyethylene ether in mixture B and stir Stand still for 10 minutes after 3min to o...

Embodiment 2

[0033] Embodiment 2: 25 parts of the water mass fraction component, 5 parts of the carbon black mass fraction component, 3 parts of the acetate resin mass fraction component, and 5 parts of the mass fraction component of the wetting and dispersing agent are added to the reaction In the kettle, the stirring speed of water, carbon black, acetate resin and wetting and dispersing agent was 80r / min, the temperature was 25°C, and the stirring time was 6min to prepare mixture A;

[0034] Mix the raw materials, add the water-based pigment to the mixture A, control the stirring speed at 50r / min, and disperse the water-based pigment into the mixture A to prepare the mixture B;

[0035] Then add alkylphenol formaldehyde resin polyoxyethylene ether in mixture B, wherein the mass fraction component of alkylphenol formaldehyde resin polyoxyethylene ether is 40 parts, add alkylphenol formaldehyde resin polyoxyethylene ether in mixture B and stir for 5min After standing still for 15min, mixtu...

Embodiment 3

[0037] Embodiment 3: 35 parts of water mass fraction components, 10 parts of carbon black mass fraction components, 5 parts of acetate-based resin mass fraction components, and 9 parts of mass fraction components of wetting and dispersing agent are added to the reaction In the kettle, the stirring speed of water, carbon black, acetate resin and wetting and dispersing agent was 120r / min, the temperature was 35°C, and the stirring time was 8min to prepare mixture A;

[0038] Then the raw materials are mixed, the water-based pigment is added to the mixture A, and the stirring speed is controlled at 90r / min to disperse the water-based pigment into the mixture A to prepare the mixture B;

[0039] Next, add alkylphenol formaldehyde resin polyoxyethylene ether in mixture B, wherein the mass fraction component of alkylphenol formaldehyde resin polyoxyethylene ether is 60 parts, add alkylphenol formaldehyde resin polyoxyethylene ether in mixture B and stir Stand still for 24min after 8...

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PUM

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Abstract

The invention provides a production method of a steel waste heat blackening agent. The method comprises the following steps: adding required water, carbon black, acetate resin and a wetting dispersantinto a reaction kettle, and stirring the water, the carbon black, the acetate resin and the wetting dispersant at a stirring rate of 50-120 r/min at the temperature of 20-35 DEG C for 5-8min so as toobtain a mixture A; and mixing raw materials, namely adding a water-based pigment into the mixture A, and dispersing the water-based pigment into the mixture A at a controlled stirring speed of 30-90r/min to obtain a mixture B. Compared with existing waste heat blackening agents, the blackening agent of the invention can form a compact double-layer blackening film on the surface of a workpiece,and the double-layer blackening film has high corrosion resistance, so that the corrosion resistance of the workpiece is greatly improved; and in addition, inorganic components and organic componentsused in the blackening agent do not pollute the environment.

Description

technical field [0001] The invention relates to a method for producing a steel waste heat blackening agent, which belongs to the technical field of steel anticorrosion. Background technique [0002] In the prior art, the black process refers to the formation of a dense black protective film layer on the surface of a metal workpiece by physical or chemical methods, thereby enhancing the anti-rust ability of the workpiece and beautifying the appearance of the workpiece at the same time. According to the different film-forming principles, the blackening process can be divided into oxidation blackening, normal temperature blackening, phosphating blackening and waste heat blackening. [0003] Waste heat blackening is to use the waste heat of the workpiece during heat treatment or other processing to make the steel workpiece form a black polymer resin film on the surface at the moment of contact with the blackening liquid, which is firmly bonded and not easy to fall off. The proc...

Claims

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Application Information

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IPC IPC(8): C09D171/02C09D201/08C09D7/61C09D5/08C09D7/63
CPCC09D5/08C09D171/02C09D7/61C09D7/63C08L101/08C08K13/02C08K3/04C08K5/41C08K5/54C08K5/10
Inventor 华家庆
Owner 镇江市乐嘉生物科技有限公司
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