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Low-temperature cured resin and curing process thereof

A low-temperature curing resin and low-temperature technology, applied in the field of low-temperature curing resin, can solve the problems of poor mechanical properties of cured products, difficulty in meeting engineering technology, and high cross-linking density, and achieve excellent mechanical properties, easy curing process, and low curing temperature Effect

Inactive Publication Date: 2020-08-28
滁州市全丰物资有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, it contains a large number of epoxy groups inside. After curing, the crosslinking density is high, the internal stress is high, and the mechanical properties of the cured product are poor. Therefore, it is difficult to meet the requirements of engineering technology, and its application is subject to certain restrictions.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A low-temperature curing resin, the raw materials of which are as follows in parts by weight: 160 parts of low-temperature curing polyester resin, 165 parts of epoxy resin mixture, 115 parts of titanium dioxide, 6 parts of toughening agent, 10 parts of curing agent, and 3 parts of accelerator 6 parts and 6 parts of diluent, the curing agent is composed of the following raw materials: 40% of 2-ethyl-4-methylimidazole, 30% of oxalic acid, 10% of glutaraldehyde, and 20% of polyallylamine.

[0019] Specifically, the epoxy resin mixture includes nano-modified bisphenol A epoxy resin, novolac epoxy resin and glycidylamine epoxy resin mixed in a ratio of 3:2:5.

[0020] Specifically, the toughening agent is amino-terminated nitrile rubber.

[0021] Specifically, the amino-terminated nitrile rubber needs to be crushed and passed through a 20-30 μm sieve.

[0022] Specifically, the solvent is a mixture of dichloromethane, toluene and xylene, and the diluent is a mixture of trie...

Embodiment 2

[0029] A low-temperature curing resin, the raw materials of which are as follows in parts by weight: 170 parts of low-temperature curing polyester resin, 170 parts of epoxy resin mixture, 125 parts of titanium dioxide, 7 parts of toughening agent, 25 parts of curing agent, and 5 parts of accelerator 15 parts of diluent, the curing agent is composed of the following raw materials: 2-ethyl-4-methylimidazole 42%, oxalic acid 24%, glutaraldehyde 10%, polyallylamine 24%.

[0030] Specifically, the epoxy resin mixture includes nano-modified bisphenol A epoxy resin, novolac epoxy resin and glycidylamine epoxy resin mixed in a ratio of 3:2:5.

[0031] Specifically, the toughening agent is amino-terminated nitrile rubber, carboxyl-terminated nitrile rubber, and epoxy-terminated nitrile rubber.

[0032] Specifically, the amino-terminated nitrile rubber, carboxyl-terminated nitrile rubber, and epoxy-terminated nitrile rubber need to be pulverized and passed through a 20-30 μm sieve.

[...

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PUM

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Abstract

The invention discloses a low-temperature cured resin. The raw materials comprise the following components in parts by weight: 160-170 parts of low-temperature cured polyester gum, 165-170 parts of epoxy resin mixture, 115-125 parts of titanium dioxide, 6-7 parts of a toughening agent, 10-25 parts of a curing agent, 1-5 parts of an accelerant and 6-15 parts of a diluent, wherein the curing agent is prepared from the following raw materials: 40%-50% of 2-ethyl-4-methylimidazole, 24%-36% of oxalic acid, 10%-13% of glutaraldehyde and 20%-30% of polyallylamine. According to the low-temperature cured resin and the curing process thereof, the toughening agent is inserted into a cured product to realize a good dispersion state so that the toughness can be improved, and the elasticity modulus canbe maintained; the 2-ethyl-4-methylimidazole component in the curing agent can be cured at a relatively low temperature to obtain a cured product with excellent heat resistance, and the cured producthas excellent mechanical properties; the curing temperature is low, and rapid curing can be achieved at the temperature of 45-55 DEG C; the produced low-temperature cured resin has lower requirementson the use environment, and is excellent in mechanical property, and the curing process is simple and easy to implement.

Description

technical field [0001] The invention relates to the technical field of low-temperature curing resins, in particular to a low-temperature curing resin and its curing process. Background technique [0002] As a thermosetting resin, resin has good electrical insulation, chemical stability, cohesiveness, processability and other characteristics, so it is widely used in construction, machinery, electronics, aerospace and other fields. However, it contains a large number of epoxy groups inside. After curing, the crosslinking density is high, the internal stress is high, and the mechanical properties of the cured product are poor. Therefore, it is difficult to meet the requirements of engineering technology, and its application is limited. Contents of the invention [0003] The purpose of the present invention is to solve the shortcomings in the prior art, and propose a low-temperature curing resin and its curing process. [0004] In order to achieve the above object, the presen...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L67/00C08L63/00C08L63/04C08L15/00C08K3/22C08K5/3445C08K5/092C08K5/07C08K13/02
CPCC08K2003/2241C08L67/00C08L2201/08C08L2205/025C08L2205/035C08L63/00C08L63/04C08L15/00C08K3/22C08K5/3445C08K5/092C08K5/07C08K13/02
Inventor 徐晶
Owner 滁州市全丰物资有限公司
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