Plant extraction and purification process

A plant extraction and process technology, applied in the direction of sugar derivatives, sugar derivatives, organic chemistry, etc., can solve problems such as bitter taste of plant extracts, can not remove the bitter taste well, and achieve environmental friendliness and product safety , the effect of improving the purity

Active Publication Date: 2020-09-04
ZHEJIANG JIANFENG HEALTH TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The purity of plant extracts is a key indicator for identifying the quality of plant extracts. However, in the process of plant extraction, impurities such as insoluble particles, tannins, and proteins in plants are often extracted, especially the presence of tannins. Affects the purity of plant

Method used

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  • Plant extraction and purification process
  • Plant extraction and purification process

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Example Embodiment

[0030] Example one

[0031] Preparation of modified nano titanium dioxide

[0032] Mix 2ml of 3-aminopropyltriethoxysilane and 100ml of absolute ethanol, add 12g of nano-titanium dioxide, stir and react under airtight conditions for 20h, after the reaction is completed, vacuum dry, mill, and ultrasonically disperse in 50ml volume fraction In a 2% glutaraldehyde solution, the reaction was continuously stirred for 22 hours under airtight conditions, filtered and dried, and then added to 100ml of 2wt% sulfonated chitosan solution. The reaction was stirred for 3 hours at a stirring speed of 800r / min, and the reaction was completed. Filter and dry to obtain modified nano titanium dioxide.

[0033] Preparation of modified polyvinyl alcohol

[0034] Add polyvinyl alcohol to 50ml of 20mM phosphate buffer saline solution, magnetically stir until it is completely dissolved to obtain a 5mg / mL polyvinyl alcohol solution, add 1.93g of N-hydroxysuccinimide, continue stirring for 30min under a nitr...

Example Embodiment

[0046] Example two

[0047] Preparation of modified nano titanium dioxide

[0048] Mix 2ml of 3-aminopropyltriethoxysilane and 100ml of absolute ethanol, add 15g of nano-titanium dioxide, stir and react under airtight conditions for 21h. After the reaction is complete, vacuum dry, mill, and ultrasonically disperse in 50ml volume fraction In a 2% glutaraldehyde solution, the reaction is continuously stirred for 20 hours under airtight conditions, filtered and dried, and then added to 100ml of 2wt% sulfonated chitosan solution. The reaction is stirred for 4 hours at a stirring speed of 800r / min, and the reaction is complete. Filtering and drying to obtain modified nano titanium dioxide.

[0049] Preparation of modified polyvinyl alcohol

[0050] Add polyvinyl alcohol to 50ml of 20mM phosphate buffer salt solution, magnetically stir until it is completely dissolved to obtain a 6mg / mL polyvinyl alcohol solution, add 1.61g of N-hydroxysuccinimide, continue to stir for 30min under a nitrog...

Example Embodiment

[0061] Example three

[0062] Preparation of modified nano titanium dioxide

[0063] Mix 2ml of 3-aminopropyltriethoxysilane and 100ml of absolute ethanol, add 10g of nano-titanium dioxide, stir and react under airtight conditions for 18h, after the reaction is complete, vacuum dry, mill, and ultrasonically disperse in 50ml volume fraction In a 2% glutaraldehyde solution, the reaction was continuously stirred for 21 hours under airtight conditions, filtered and dried, and then added to 100ml of 2wt% sulfonated chitosan solution. The reaction was stirred for 3 hours at a stirring speed of 800r / min, and the reaction was completed. Filtering and drying to obtain modified nano titanium dioxide.

[0064] Preparation of modified polyvinyl alcohol

[0065] Add polyvinyl alcohol to 50ml of 20mM phosphate buffer saline solution, magnetically stir until it is completely dissolved to obtain a 8mg / mL polyvinyl alcohol solution, add 1.79g of N-hydroxysuccinimide, continue to stir for 30min under ...

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Abstract

The invention discloses a plant extraction and purification process, and relates to the technical field of plant extraction. The extraction and purification process comprises the following steps: cleaning, drying and crushing a to-be-extracted plant, adding a 50-70% ethanol solution, carrying out alcohol extraction to obtain an alcohol extracting solution, feeding the alcohol extracting solution into a macroporous resin column, after adsorption is completed, washing with deionized water with the volume 1-2 times that of the column to remove impurities, eluting with a 60-70% ethanol solution, collecting eluent, concentrating under reduced pressure to obtain extract with the relative density of 1.10-1.15, adding ethanol into the obtained extract, stirring, fully dissolving, standing, filtering, collecting filtrate to obtain purified extracting solution, and filtering the purified extracting solution with an ultrafiltration membrane to obtain a refined extracting solution. The plant extraction and purification process can effectively separate impurities in an extracting solution so as to improve the purity of active ingredients, and does not use any organic solvent in the whole extraction process, so that the product is safer and more environment-friendly.

Description

technical field [0001] The invention relates to the technical field of plant extraction, in particular to a plant extraction and purification process. Background technique [0002] With the development of our country's economy and the improvement of people's living standards, people are increasingly recognizing the life philosophy of "pursuing nature and advocating nature". The health care effect of natural food has attracted much attention, and the plant extract industry has become the fastest growing domestically in the past 10 years. one of the industries. [0003] Plant extraction mainly extracts active substances in plants. Different active substances have different effects, such as: anti-aging, anti-fatigue, anti-radiation, anti-hypoxia, anti-virus and anti-tumor, anti-peroxidation, etc., and its effect The quality of the effect is often directly related to the purity of the plant extract. The purity of plant extracts is a key indicator for identifying the quality of...

Claims

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Application Information

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IPC IPC(8): B01D61/14B01D67/00B01D69/02B01D69/12B01D71/34B01D71/38C07H1/08C07H15/18
CPCB01D61/145B01D71/38B01D71/34B01D69/02B01D69/12B01D67/0002C07H15/18C07H1/08B01D2325/48B01D2323/39B01D2325/36
Inventor 杨浩赵春全陈安平
Owner ZHEJIANG JIANFENG HEALTH TECH
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