Plant extraction and purification process
A plant extraction and process technology, applied in the direction of sugar derivatives, sugar derivatives, organic chemistry, etc., can solve problems such as bitter taste of plant extracts, can not remove the bitter taste well, and achieve environmental friendliness and product safety , the effect of improving the purity
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[0030] Example one
[0031] Preparation of modified nano titanium dioxide
[0032] Mix 2ml of 3-aminopropyltriethoxysilane and 100ml of absolute ethanol, add 12g of nano-titanium dioxide, stir and react under airtight conditions for 20h, after the reaction is completed, vacuum dry, mill, and ultrasonically disperse in 50ml volume fraction In a 2% glutaraldehyde solution, the reaction was continuously stirred for 22 hours under airtight conditions, filtered and dried, and then added to 100ml of 2wt% sulfonated chitosan solution. The reaction was stirred for 3 hours at a stirring speed of 800r / min, and the reaction was completed. Filter and dry to obtain modified nano titanium dioxide.
[0033] Preparation of modified polyvinyl alcohol
[0034] Add polyvinyl alcohol to 50ml of 20mM phosphate buffer saline solution, magnetically stir until it is completely dissolved to obtain a 5mg / mL polyvinyl alcohol solution, add 1.93g of N-hydroxysuccinimide, continue stirring for 30min under a nitr...
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[0046] Example two
[0047] Preparation of modified nano titanium dioxide
[0048] Mix 2ml of 3-aminopropyltriethoxysilane and 100ml of absolute ethanol, add 15g of nano-titanium dioxide, stir and react under airtight conditions for 21h. After the reaction is complete, vacuum dry, mill, and ultrasonically disperse in 50ml volume fraction In a 2% glutaraldehyde solution, the reaction is continuously stirred for 20 hours under airtight conditions, filtered and dried, and then added to 100ml of 2wt% sulfonated chitosan solution. The reaction is stirred for 4 hours at a stirring speed of 800r / min, and the reaction is complete. Filtering and drying to obtain modified nano titanium dioxide.
[0049] Preparation of modified polyvinyl alcohol
[0050] Add polyvinyl alcohol to 50ml of 20mM phosphate buffer salt solution, magnetically stir until it is completely dissolved to obtain a 6mg / mL polyvinyl alcohol solution, add 1.61g of N-hydroxysuccinimide, continue to stir for 30min under a nitrog...
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[0061] Example three
[0062] Preparation of modified nano titanium dioxide
[0063] Mix 2ml of 3-aminopropyltriethoxysilane and 100ml of absolute ethanol, add 10g of nano-titanium dioxide, stir and react under airtight conditions for 18h, after the reaction is complete, vacuum dry, mill, and ultrasonically disperse in 50ml volume fraction In a 2% glutaraldehyde solution, the reaction was continuously stirred for 21 hours under airtight conditions, filtered and dried, and then added to 100ml of 2wt% sulfonated chitosan solution. The reaction was stirred for 3 hours at a stirring speed of 800r / min, and the reaction was completed. Filtering and drying to obtain modified nano titanium dioxide.
[0064] Preparation of modified polyvinyl alcohol
[0065] Add polyvinyl alcohol to 50ml of 20mM phosphate buffer saline solution, magnetically stir until it is completely dissolved to obtain a 8mg / mL polyvinyl alcohol solution, add 1.79g of N-hydroxysuccinimide, continue to stir for 30min under ...
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