Preparation method of preservative film for preserving tender ginger
A technology of fresh-keeping film and tender ginger, applied in the field of fresh-keeping packaging materials, can solve the problems of easy water loss, reduced brittle and tender quality, single function, etc., achieve high water absorption performance and antibacterial performance, improve strength and toughness, and graft conversion rate. high effect
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Embodiment 1
[0053] A method for preparing a preservative film for preserving young ginger, characterized in that it includes chitosan grafting reaction, copolymer synthesis of ethylene-vinyl acetic acid-chitosan graft product, nano-silica modification and fresh-keeping film preparation;
[0054] Wherein, the concrete steps of chitosan grafting reaction are:
[0055] a 1 , first add 60 parts by weight of toluene in the reactor, then use nitrogen to replace the air in the reactor, start stirring under nitrogen protection atmosphere, then add 1 part by weight of chitosan in toluene; use nitrogen in the stirring process Protection, and the temperature is controlled at 110°C by means of oil bath heating;
[0056] b 1 1. Add a mixture of concentrated sulfuric acid and nitric acid as a catalyst in the chitosan toluene mixed solution, wherein the mass ratio of concentrated sulfuric acid and nitric acid (for the concentrated sulfuric acid and nitric acid of the commonly used concentration on th...
Embodiment 2
[0073] A method for preparing a preservative film for preserving young ginger, characterized in that it includes chitosan grafting reaction, copolymer synthesis of ethylene-vinyl acetic acid-chitosan graft product, nano-silica modification and fresh-keeping film preparation;
[0074] Wherein, the concrete steps of chitosan grafting reaction are:
[0075] a 1 , first add 80 parts by weight of toluene in the reactor, then use nitrogen to replace the air in the reactor, start stirring under nitrogen protection atmosphere, then add 6 parts by weight of chitosan in toluene; use nitrogen in the stirring process protection, and the temperature is controlled at 115°C by means of oil bath heating;
[0076] b 1 1. Add a mixture of concentrated sulfuric acid and nitric acid as a catalyst in the chitosan toluene mixed solution, wherein the mass ratio of concentrated sulfuric acid and nitric acid (being the concentrated sulfuric acid and nitric acid of the usual concentration on the mar...
Embodiment 3
[0093] A method for preparing a preservative film for preserving young ginger, characterized in that it includes chitosan grafting reaction, copolymer synthesis of ethylene-vinyl acetic acid-chitosan graft product, nano-silica modification and fresh-keeping film preparation;
[0094] Wherein, the concrete steps of chitosan grafting reaction are:
[0095] a 1 1. First add 100 parts by weight of toluene to the reactor, then use nitrogen to replace the air in the reactor, start stirring under nitrogen protection atmosphere, then add 10 parts by weight of chitosan in toluene; use nitrogen in the stirring process protection, and the temperature is controlled at 120°C by means of oil bath heating;
[0096] b 1 1. Add a mixture of concentrated sulfuric acid and nitric acid as a catalyst in the chitosan toluene mixed solution, wherein the mass ratio of concentrated sulfuric acid and nitric acid (being the concentrated sulfuric acid and nitric acid of the usual concentration on the ...
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