Silane modified polycarboxylate superplasticizer, preparation method thereof, concrete admixture using superplasticizer, and preparation method of concrete admixture
A technology of concrete admixture and silane modification, which is applied in the fields of silane-modified polycarboxylate water reducer, concrete admixture, and chemical admixture. The admixture system is stable, maintains workability, and the effect of system stability
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Embodiment 1
[0059] 1. Silane-modified polycarboxylate water reducer and its preparation method
[0060] In this example, a silane-modified polycarboxylate water-reducer was prepared. The raw materials used include: polyoxyethylene ether 10%, acrylic acid 32%, γ-methacryloxypropyl trimethoxysilane 1.8% by mass percentage %, ammonium persulfate 0.35%, 3-mercaptoacetic acid 0.18%, and the balance is deionized water.
[0061] Concrete preparation method comprises the following steps:
[0062] (1) Mix 10% (mass percentage, the same below) polyoxyethylene ether with a small amount of deionized water, put it in a three-necked flask and place it in a water bath, stir and pre-dissolve the mixture at a temperature of 30°C, and set aside;
[0063] (2) Mix 0.35% initiator ammonium persulfate, 32% acrylic acid and deionized water to prepare material A; 0.18% chain transfer agent 3-mercaptoacetic acid and deionized water to prepare material B; 1.8% monomer γ-formazol Acryloyloxypropyltrimethoxysilan...
Embodiment 2
[0077] Others are the same as in Example 1, except that n=20.
Embodiment 3
[0079] Others are the same as in Example 1, except that n=50.
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