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Anti-floating fiber agent and anti-floating fiber polypropylene reinforced composite material

A technology of polypropylene reinforcement and anti-floating fiber agent, which is applied in the field of anti-floating fiber agent and a kind of anti-floating fiber polypropylene reinforced composite material, which can solve the problems of affecting the mechanical properties of products, the inability to apply dark-colored products, and precipitation and stickiness.

Inactive Publication Date: 2020-10-23
KINGFA SCI & TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In many current studies, some scholars use anti-floating fiber masterbatches, such as CN108912514, which uses glass fiber and PB-1 as anti-floating fiber masterbatches and then adds them to the finished product, so that the glass fiber in the masterbatch has undergone a second pass and the retention length will be reduced. Reduce and affect the mechanical properties of the product; such as CN 103756014 B uses zinc oxide as anti-floating fiber masterbatch, this anti-floating fiber masterbatch is white, and cannot be applied to dark-colored products
In addition, some scholars add anti-floating fiber agents in products, and the types of anti-floating fiber agents are also various, such as CN 107254104 A using high-melt index PP (MFR>500g / 10min), ethylene bisstearic acid amide dispersion dispersant and TAF lubricant, but ethylene bis stearic acid amide dispersant and TAF are small molecules that may cause stickiness due to precipitation

Method used

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  • Anti-floating fiber agent and anti-floating fiber polypropylene reinforced composite material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0065] An embodiment of the anti-floating fiber polypropylene reinforced composite material of the present invention, the anti-floating fiber polypropylene reinforced composite material described in this embodiment is prepared by the following method:

[0066] Step 1: Preparation of purified PB-1-g-MAH

[0067] a. First weigh 3 parts of monomer maleic anhydride (MAH), 0.2 parts of initiator di-tert-butyl peroxide (DTBP), 1 part of co-monomer α-methylstyrene (AMS), 0.5 parts of co-monomer The bulk 1-octene (1-Octene) was dissolved in 30 parts of acetone at 30°C to obtain a mixed solution A for use.

[0068] b. Add the above mixed solution A to 80 parts of PB-1PB0800M and mix and stir evenly at room temperature. After the acetone is completely volatilized, add it to a twin-screw extruder for melt extrusion grafting reaction to obtain PB-1-g-MAH crude compounds. Wherein, the temperature of the twin-screw extruder is 130-150°C.

[0069] c. Take 1 part of PB-1-g-MAH crude produc...

Embodiment 2

[0073] An embodiment of the anti-floating fiber polypropylene reinforced composite material of the present invention, the anti-floating fiber polypropylene reinforced composite material described in this embodiment is prepared by the following method:

[0074] Step 1: Preparation of purified PB-1-g-MAH

[0075] a. First weigh 8 parts of monomer maleic anhydride (MAH), 0.5 parts of initiator di-tert-butyl peroxide (DTBP), 3 parts of co-monomer α-methylstyrene (AMS), 1.5 parts of co-monomer The bulk 1-octene (1-Octene) was dissolved in 50 parts of acetone at 45°C to obtain a mixed solution A for use.

[0076] b. Add the above mixed solution A to 100 parts of PB-1PB0401M and mix and stir evenly at room temperature. After the acetone is completely volatilized, add it to a twin-screw extruder for melt extrusion grafting reaction to obtain PB-1-g-MAH crude compounds. Wherein, the temperature of the twin-screw extruder is 130-150°C.

[0077] c. Take 1 part of PB-1-g-MAH crude prod...

Embodiment 3

[0081] An embodiment of the anti-floating fiber polypropylene reinforced composite material of the present invention, the anti-floating fiber polypropylene reinforced composite material described in this embodiment is prepared by the following method:

[0082] Step 1: Preparation of purified PB-1-g-MAH

[0083] a. First weigh 4.6 parts of monomer maleic anhydride (MAH), 0.28 parts of initiator di-tert-butyl peroxide (DTBP), 1.6 parts of co-monomer α-methylstyrene (AMS), 0.7 parts of co-monomer The bulk 1-octene (1-Octene) was dissolved in 34 parts of acetone at 33°C to obtain a mixed solution A for use.

[0084] b. Add the above mixed solution A to 84 parts of PB-1PB0401M and mix and stir evenly at room temperature. After the acetone is completely volatilized, add it to a twin-screw extruder for melt extrusion grafting reaction to obtain PB-1-g-MAH crude compounds. Wherein, the temperature of the twin-screw extruder is 130-150°C.

[0085] c. Take 1 part of PB-1-g-MAH crude ...

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Abstract

The invention discloses an anti-floating fiber agent and a preparation method thereof. Meanwhile, the invention also discloses an anti-floating fiber polypropylene reinforced composite material. The anti-floating fiber polypropylene reinforced composite material comprises the following components in parts by weight, 35-90 parts of polypropylene, 20-50 parts of glass fibers, 5-15 parts of the anti-floating fiber agent and 0.2-0.6 part of an antioxidant, the polypropylene comprises polypropylene A, and the melt flow rate of the polypropylene A at 230 DEG C and 2.16 kg is 1000-1500g / 10min. By using the polypropylene A and the anti-floating fiber agent, the glass fiber can be better wrapped and infiltrated, so that the appearance anti-floating fiber effect is good; in addition, the invention also discloses a preparation method of the anti-floating fiber polypropylene reinforced composite material.

Description

technical field [0001] The invention relates to the field of polymer material modification, in particular to an anti-floating fiber agent and an anti-floating fiber polypropylene reinforced composite material. Background technique [0002] Glass fiber reinforced polypropylene (GFRPP) has the advantages of high rigidity, high impact, good fatigue creep resistance, short molding cycle, and recyclability, which largely solves a series of shortcomings such as low rigidity and poor fatigue creep of pure PP. After being put into use in the 1970s, it has been widely used in many fields such as home appliances, electronic appliances, construction industry, aerospace, ships and automobiles. However, in terms of engineering applications, the phenomenon of glass fiber exposure greatly limits the use of GFRPP materials. [0003] In recent years, with the improvement of the use environment and aesthetic requirements of polymer materials, people have put forward higher requirements for t...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08F255/10C08F222/06C08F212/12C08F210/14C08L23/12C08L51/06C08K7/14C08K5/134C08K5/526B29B9/06
CPCC08F255/10C08L23/12B29B9/06C08L2205/03C08L2205/025C08F222/06C08L51/06C08K7/14C08K5/1345C08K5/526
Inventor 俞飞罗睿黄险波叶南飚吴国峰赖昂丁正亚杨波罗忠富
Owner KINGFA SCI & TECH CO LTD
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