Gas-sensing nanomaterials based on carbon particle-modified mesoporous iron oxide nanorod structure, preparation process and application
An iron oxide nanometer and nanomaterial technology, which is applied in the field of semiconductor nanomaterial preparation and gas sensing applications, can solve problems such as damage to human health, achieve long-term stability and improve service life, overcome the high complexity of the preparation process, and improve the response. /restore speed effect
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Embodiment 1
[0037] (1) Add 0.32 g of F127 and 0.358 g of ferric chloride hexahydrate into 30 mL of deionized water and mix well to obtain mixed solution A;
[0038] (2) After stirring the mixed solution A prepared in step (1) for 1 hour, inject 1.2 mL of anhydrous acetic acid to obtain a mixed solution B;
[0039] (3) After stirring the mixed solution B prepared in step (2) for 1 hour, 0.12 g of 2-aminoterephthalic acid solid was added to obtain a mixed solution C;
[0040] (4) After stirring the mixed solution C prepared in step (3) for 2 hours, pour it into a hydrothermal kettle as a precursor solution, conduct solvothermal reaction at 110 ° C for 24 hours, wash it with ethanol for several times and blow dry after completion. , the self-sacrificial template material Fe-MOF nanorods were obtained, and the SEM characterization images are as follows figure 2 It can be seen that the Fe-MOF nanorods have an average diameter of about 86 nm and an average length of about 540 nm;
[0041] (5) ...
Embodiment 2
[0046] Similar to Example 1, the difference is that the calcination temperature during one-step calcination is 350°C. The SEM characterization of the obtained carbon particle-modified mesoporous iron oxide nanorods is shown in Fig. Figure 7 As shown, the average diameter of the mesoporous iron oxide nanorods is about 52 nm, the average length is about 436 nm, the average mesopore diameter is about 5 nm, and the average diameter of the carbon particles is about 5 nm. , the average diameter and average length of the carbon particle-modified mesoporous iron oxide nanorods obtained by calcination decreased accordingly, the mesopore size increased, while the average size of carbon particles decreased and the surface distribution concentration decreased. The mesoporous iron oxide nanorods decorated with carbon particles obtained by calcination at 350 °C were also tested for acetone gas sensing performance. The results are as follows: Figure 8 As shown, although the response is sl...
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