Polyurethane-based ionic liquid perfusion coating prefabricated liquid, preparation method thereof and ionic liquid perfusion coating
An ionic liquid and liquid infusion technology, applied in polyurea/polyurethane coatings, coatings, etc., can solve the problems of cumbersome steps, expensive preparation of devices, uncleanness and environmental protection, etc., and achieve the effects of simple operation, broad market prospects and low price.
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Embodiment 1
[0046] The embodiment of the present application provides the first ionic liquid perfusion coating, the method comprising:
[0047] 1. Weigh 0.05g of thermoplastic polyurethane TPU and 0.5g of 1-butyl-3-methylimidazolium hexafluorophosphate [BMIM][PF 6 ] was added to a 5mL reagent bottle;
[0048] 2. Then, gradually heat in the oil bath, stir at a speed of 300rpm, heat to 180°C and keep the temperature for 3 hours to completely dissolve the polyurethane TPU in the ionic liquid [BMIM][PF 6 ] to form a homogeneous polyurethane-based ionic liquid perfusion coating prefabricated solution, place the polyurethane-based ionic liquid perfused coating prefabricated solution on a glass plate, and use a scraper to quickly scrape out a 1mm thick solution layer. After standing for 30s, the polyurethane-based ionic liquid perfusion coating prefabricated liquid cooled naturally and phase separation occurred to form the ionic liquid perfusion coating.
Embodiment 2
[0050] The embodiment of the present application provides a second ionic liquid perfusion coating, the method comprising:
[0051] 1. Weigh 0.2g of polyurethane TPU and 1g of 1-octyl-3-methylimidazolium hexafluorophosphate [OMIM][PF 6 ], added to the reagent bottle of 5mL;
[0052] 2. Then, gradually heat in the oil bath, stir at a speed of 300rpm, heat to 180°C and keep the temperature for 3 hours to completely dissolve the polyurethane TPU in the ionic liquid [OMIM][PF 6 ] The polyurethane-based ionic liquid perfusion coating prefabricated solution formed in ], put the polyurethane-based ionic liquid perfused coating prefabricated solution on a glass plate, and use a scraper to quickly scrape out a 1mm thick solution layer. After standing for 30s, the polyurethane-based ionic liquid perfusion coating prefabricated liquid cooled naturally and phase separation occurred to form the ionic liquid perfusion coating.
Embodiment 3
[0054] The embodiment of the present application provides a third ionic liquid perfusion coating, the method comprising:
[0055] 1. Weigh 0.2g of thermoplastic polyurethane TPU and 1g of 1-decyl-3-methylimidazolium hexafluorophosphate [DMIM][PF 6 ] was added to a 5mL reagent bottle;
[0056] 2. Then, gradually heat in the oil bath, stir at a speed of 300rpm, heat to 200°C and keep the temperature for 2 hours to completely dissolve the polyurethane TPU in the ionic liquid [DMIM][PF 6 ] to form a homogeneous polyurethane-based ionic liquid perfusion coating prefabricated solution, place the polyurethane-based ionic liquid perfused coating prefabricated solution on a glass plate, and use a scraper to quickly scrape out a 1mm thick solution layer. After standing for 30s, the polyurethane-based ionic liquid perfusion coating prefabricated liquid cooled naturally and phase separation occurred to form the ionic liquid perfusion coating.
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