Method for preparing silver-nickel-tin-oxide-doped electric contact material on basis of ball-milling method
An electrical contact material, tin oxide technology, applied in circuits, electrical switches, electrical components and other directions, can solve the problems of poor electrical conductivity of electrical contact materials, long material preparation period, difficult to achieve industrialization, etc. Wear properties and anti-welding properties, control of growth and the effect of agglomeration
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Embodiment 1
[0063] Step 1. Weigh tin oxide powder, other oxide powders and grinding balls respectively, and process the mixed powder symmetrically taken by high-energy ball milling technology to obtain preliminary mixed oxide powder A. The specific steps are:
[0064] 1.1) Weigh nano tin oxide powder, La 2 o 3 And stainless steel grinding balls, nano tin oxide powder, La 2 o 3 The mass ratio to the grinding ball is 5:1:100;
[0065] 1.2) Add the oxide powder weighed in step 1.1) together with stainless steel balls into the ball milling jar, then add absolute ethanol to the ball milling jar, add 3ml of absolute ethanol to each gram of oxide powder, start the ball mill for ball milling Treatment, ball milling time 2h;
[0066] In order to ensure the ball milling effect, during the ball milling process, the total volume of nano-oxide powder, absolute ethanol and stainless steel balls accounts for 40% of the ball milling tank volume;
[0067] 1.3) Place the mixed oxide powder obtained af...
Embodiment 2
[0084] Step 1. Weigh tin oxide powder, other oxide powders and bearing steel grinding balls respectively, and process the mixed powder symmetrically taken by high-energy ball milling technology to obtain preliminary mixed oxide powder A. Specifically, follow the steps below:
[0085] 1.1) Weigh nano tin oxide powder, CuO powder and bearing steel grinding ball respectively, the mass ratio of nano tin oxide powder, CuO powder and grinding ball is 6:2:103;
[0086] 1.2) Add the oxide powder weighed in step 1.1) together with the bearing steel grinding balls into the ball milling jar, then add absolute ethanol to the ball milling jar, add 4ml of absolute ethanol to each gram of oxide powder, start the ball mill Ball milling treatment, ball milling time 3h;
[0087] In order to ensure the ball milling effect, during the ball milling process, the total volume of nano-oxide powder, absolute ethanol and bearing steel balls accounts for 50% of the ball milling tank volume;
[0088] 1....
Embodiment 3
[0105] Step 1, weigh tin oxide powder, La 2 o 3 The powder and zirconia grinding balls are treated with the mixed powder symmetrically taken by high-energy ball milling technology to obtain the preliminary mixed oxide powder A, which is specifically implemented according to the following steps:
[0106] 1.1) Weigh nano tin oxide powder, La 2 o 3 powder and zirconia grinding balls, nano tin oxide powder, La 2 o 3 The mass ratio of powder to zirconia balls is 8:5:110;
[0107] 1.2) Add the oxide powder weighed in step 1.1) together with the zirconia balls into the ball milling jar, then add absolute ethanol to the ball milling jar, add 5ml of absolute ethanol for each gram of oxide powder, start the ball mill Ball milling treatment, ball milling time 4h;
[0108] In order to ensure the ball milling effect, during the ball milling process, the total volume of nano-oxide powder, absolute ethanol and zirconia balls accounts for 60% of the ball milling tank volume;
[0109] 1...
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