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Compound, organic electroluminescent device and electronic device

A compound and chemical formula technology, applied in the field of organic electroluminescent materials, can solve the problems of short luminous life and low luminous efficiency, and achieve the effects of increasing recombination rate, improving efficiency performance, and reducing π-π stacking

Active Publication Date: 2020-11-20
SHAANXI LIGHTE OPTOELECTRONICS MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the current organic electroluminescent materials still have the problems of short luminous lifetime and low luminous efficiency.

Method used

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  • Compound, organic electroluminescent device and electronic device
  • Compound, organic electroluminescent device and electronic device
  • Compound, organic electroluminescent device and electronic device

Examples

Experimental program
Comparison scheme
Effect test

Synthetic example

[0236]In the synthesis examples described below, all temperatures are in degrees Celsius unless otherwise stated. Some reagents were purchased from commercial suppliers such as Aldrich Chemical Company, Arco Chemical Company and Alfa Chemical Company, and some intermediates that could not be directly purchased were prepared from commercially available raw materials through simple reactions. Unless otherwise stated, they were used without further purification. The rest of the conventional reagents are from Shantou Xilong Chemical Factory, Guangdong Guanghua Chemical Reagent Factory, Guangzhou Chemical Reagent Factory, Tianjin Haoyuyu Chemical Co., Ltd., Tianjin Fuchen Chemical Reagent Factory, Wuhan Xinhuayuan Technology Development Co., Ltd., Qingdao Tenglong It can be purchased from Chemical Reagent Co., Ltd. and Qingdao Ocean Chemical Factory. Anhydrous tetrahydrofuran, dioxane, toluene, ether and other anhydrous solvents are obtained by reflux drying of metal sodium. The r...

preparation example 1-13

[0243] 1. Synthesis of intermediate a-1

[0244]

[0245] 2-Bromo-4-chloro-1-iodobenzene (80.0 g; 252.1 mmol), phenylboronic acid (33.8 g; 277.3 mmol), tetrakis(triphenylphosphine)palladium (5.8 g; 5.0 mmol), potassium carbonate ( 76.5g; 554.6mmol), tetrabutylammonium bromide (16.2g; 50.4mmol) were added in the flask, and a mixed solvent of toluene (640mL), ethanol (320mL) and water (160mL) was added, under nitrogen protection, the temperature was raised to 80°C, keep the temperature and stir for 8 hours; cool to room temperature, stop stirring, wash the reaction solution with water, separate the organic phase, dry with anhydrous magnesium sulfate, remove the solvent under reduced pressure, and obtain the crude product; use n-heptane as the mobile phase crude product for silica gel column After chromatographic purification, intermediate a-1 (40.5 g; yield 60%) was obtained as a light gray solid product.

[0246] Using a method similar to the synthesis of intermediate a-1, ...

preparation example 2-14

[0297] Table 9: Preparation Examples 2-14

[0298]

[0299]

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PUM

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Abstract

The invention provides an organic compound, an organic electroluminescent device and an electronic device. The chemical structure of the organic compound comprises an adamantane spirofluorene ring anda dibenzo five-membered ring, and the organic compound has an excellent energy transfer function, can be used as a luminescent layer material in an electroluminescent device, improves the efficiencyof the organic electroluminescent device and prolongs the service life of the organic electroluminescent device.

Description

technical field [0001] The invention belongs to the technical field of organic electroluminescent materials, and in particular relates to a compound, an organic electroluminescent device and an electronic device using the compound. Background technique [0002] An organic electroluminescence device, such as an organic light emitting diode (OLED), generally includes a cathode and an anode oppositely arranged, and a functional layer arranged between the cathode and the anode. The functional layer is composed of multiple organic or inorganic film layers, and generally includes an organic light-emitting layer, a hole transport layer located between the organic light-emitting layer and the anode, and an electron transport layer located between the organic light-emitting layer and the cathode. When a voltage is applied to the cathode and anode, the two electrodes generate an electric field. Under the action of the electric field, the electrons on the cathode side move to the elect...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07D405/10C07D405/14C07D409/14C07D495/04C07D307/91C07D409/04C07D409/10C07D491/048C07D333/76C07F7/08C09K11/06H01L51/54
CPCC07D405/10C07D405/14C07D409/14C07D495/04C07D307/91C07D409/04C07D409/10C07D491/048C07D333/76C07F7/0816C09K11/06C09K2211/1088C09K2211/1092C09K2211/1007C09K2211/1011C09K2211/1044C09K2211/1059C09K2211/1029C09K2211/1051H10K85/654H10K85/6576H10K85/6574H10K85/657H10K85/40H10K85/6572C07D413/10C07D405/04C07D239/70C07D251/24C07D239/26C07D471/04C07D417/10C07C15/38C07C2603/74C07C2603/40H10K85/622H10K85/615H10K2101/90H10K50/11C07B2200/05C07C13/64C07F7/0812
Inventor 郑奕奕马天天
Owner SHAANXI LIGHTE OPTOELECTRONICS MATERIAL CO LTD
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