Preparation method and application of cyanobacteria modified charcoal with high adsorption efficiency
A technology of biochar and high adsorption, applied in chemical instruments and methods, adsorption water/sewage treatment, restoration of contaminated soil, etc., can solve problems such as imperfect soil remediation technology, reduce migration and transformation risks, increase pore size, Effect of large specific surface area and porosity
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[0035] Embodiment 1: 1-1. Preparation of modified cyanobacterial biochar, the specific steps are as follows:
[0036] 1-1-1. Collect the cyanobacteria salvaged from the salvage station, dry them in a 105°C oven, pulverize them with a pulverizer, and then put them in a quartz boat and put them in a tube furnace, and carry out the process under nitrogen protection. Carbonized treatment. The heating rate was required to be 5 °C / min, the nitrogen flow rate was 50 mL / min, the heating temperature was first raised from room temperature to 300 °C, kept for 1 h, and then cooled to room temperature, and the obtained carbon material was marked as ZC300.
[0037] 1-1-2. First, the carbon material ZC300 is further pulverized by a pulverizer and passed through a 100-mesh sieve. Then the undersize was mixed with KOH in a mass ratio of 1:2, and deionized water was added to make the KOH concentration at 20%. Then, the mixture was dried in an oven at 80° C., and then placed in a tube furnace,...
Example Embodiment
[0046] Example 2:
[0047] 2-1. Preparation of modified cyanobacterial biochar, the specific steps are as follows:
[0048] 2-1-1. Put the collected blue-green algae in a freeze-drying machine to freeze-dry, pass through a 100-mesh sieve after being pulverized by a pulverizer, and put them into a tube furnace for carbonization. The heating rate is 5°C / min, and the nitrogen flow rate is 0.5L / min, the temperature was raised from room temperature to 300 °C, kept for 2 h, and then cooled to room temperature, and the obtained carbon material was marked as ZC300.
[0049] 2-1-2. First, add the carbon material ZC300 into KOH according to the mass ratio of 1:3 and mix evenly, then add deionized water to make the KOH concentration at 30%. The mixture was dried in an oven at 80 °C, then carbonized in a tube furnace, heated to 700 °C, kept for 3 h, and cooled to room temperature. The obtained carbon material was marked as KOH-ZC700.
[0050] 2-1-3. Add 40% HCl to the above-mentioned c...
Example Embodiment
[0055] Example 3:
[0056] 3-1. Preparation of modified cyanobacterial biochar, the specific steps are as follows:
[0057] 3-1-1. Collect the blue-green algae and place them in a 105°C oven to dry, then crush them with a crusher and put them into a tube furnace for carbonization treatment. The heating rate is 5°C / min, and the nitrogen flow rate is 80mL / min. The temperature was increased from room temperature to 300 °C and maintained for 1.5 h, and the obtained carbon material was marked as ZC300.
[0058] 3-1-2. Pulverize the cooled ZC300 and pass it through a 100-mesh sieve, add KOH according to the mass ratio of 1:2.5 and mix evenly, add deionized water to make the KOH concentration 30%, put it in a 90 ℃ oven to dry, and then put Carbonized in a tube furnace, heated to 700 °C, maintained for 2.5 h, cooled to room temperature, and the obtained carbon material was marked as KOH-ZC700.
[0059] 3-1-3. Add 30% HNO3 to the above cooled KOH-ZC700, shake on a shaking table for 2...
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