The present application relates to
solid waste
resource utilization technical field, disclose a kind of methods for preparing
silicon micro
powder based on chlorination waste brine
quenching slag in situ carbothermal reduction, method includes: S1, the
molten salt chlorination waste brine
quenching slag is carried out
drying and ball milling treatment, and pretreatment material is obtained;S2, pretreatment material is carried out
magnetic separation, and non-magnetic mixture is obtained;S3, after non-magnetic mixture and mixed acid are carried out acid dipping reaction,
solid-liquid separation is carried out, and the
silicon-rich filter residue containing
silicon dioxide and
elemental carbon is obtained;S4, after silicon-rich filter residue is washed and dried,
silicon dioxide and
elemental carbon in it are made to carry out carbothermal reduction reaction under
inert atmosphere, and silicon micro
powder product is obtained.The purity and
resource utilization rate of silicon micro
powder product are improved by the scheme of the present application, and high-value and clean utilization of waste water
quenching slag is realized.