A kind of external wall interface agent and preparation method thereof
An interfacial agent and wall technology, applied in coatings, rosin coatings, alginic acid coatings, etc., can solve the problems affecting the bonding performance of interfacial agents, and achieve the effects of increased adhesion, strong flexibility, and good air permeability.
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[0039] Preparation example of polyvinyl acetate emulsion
[0040] The polyvinyl alcohol in the following preparation examples was purchased from polyvinyl alcohol 1799100-27 produced by Shanghai Huihu Industrial Co., Ltd.; vinyl acetate was purchased from Jinan Mingwei Chemical Co., Ltd., with a density of 0.93g / cm 3 ; Dibutyl phthalate was purchased from Xi'an Tianmao Chemical Co., Ltd.; Butyl acrylate was purchased from Jinan Mingwei Chemical Co., Ltd.
preparation example 1
[0041] Preparation example 1: polyvinyl acetate emulsion is prepared by the following method:
[0042] ⅠWeigh 62kg of deionized water, 6kg of polyvinyl alcohol, 32kg of vinyl acetate, 0.28kg of ammonium persulfate, 0.04kg of dibutyl phthalate, 7kg of butyl acrylate, and 0.08kg of sodium bicarbonate;
[0043] ⅡPlace deionized water and polyvinyl alcohol in a reaction kettle, stir for 5 minutes at 87°C and 600 r / min, then add dibutyl phthalate and sodium bicarbonate and continue stirring for 4 minutes to obtain a stirring liquid;
[0044] Ⅲ Add ammonium persulfate, vinyl acetate, and butyl acrylate to the stirred liquid prepared by Ⅱ, and stir at a speed of 550r / min for 12min to prepare a polyvinyl acetate emulsion.
[0045] Preparation of polyvinyl alcohol solution The titanate coupling agent in the following preparation examples was purchased from Hefei Anbang Chemical Co., Ltd., model 550; the polyvinyl alcohol was purchased from Shanghai Huihu Industrial Co., Ltd. polyvinyl ...
preparation example 2
[0046] Preparation example 2: polyvinyl alcohol solution is prepared by the following method:
[0047] ①Weigh 70kg of deionized water, 3.5kg of polyvinyl alcohol, and 0.25kg of titanate coupling agent;
[0048] ②Put deionized water and polyvinyl alcohol in a reaction kettle, stir for 40 min at 85°C and 400 r / min, then add titanate coupling agent and continue stirring for 1.8 h to obtain a polyvinyl alcohol solution.
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