Silicon carbide ceramic sealing ring and preparation method thereof
A silicon carbide ceramic and sealing ring technology, which is used in engine seals, mechanical equipment, engine components, etc., can solve the problems of poor performance and low density of ceramic products, improve mechanical properties, enhance adsorption capacity, and promote mixing. Effect
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[0020] The following describes the preparation method of the silicon carbide ceramic sealing ring proposed in this application, which may include the following steps: preparing raw materials. Silicon carbide is used as the main raw material, and the first sintering aid, the second sintering aid, water reducer and other additives are introduced as auxiliary raw materials. Wherein, silicon carbide may be selected from one or a combination of nanoscale α-type silicon carbide, nanoscale β-type silicon carbide, submicron-scale α-type silicon carbide, and submicron-scale β-type silicon carbide. Wherein, the first sintering aid can be selected from amorphous carbon (carbon black), activated carbon, crystalline elemental carbon (nanoscale single-layer or multi-layer graphene and graphene oxide), carbon nanotubes, mesophase carbon microspheres, One or a combination of organic precursors of carbon, carbides, borides, nitrides, silicides and oxides of metals. Wherein, the second sinteri...
Embodiment 1
[0025] This embodiment proposes a method for preparing a silicon carbide ceramic sealing ring, which may include the following steps: preparing raw materials. Using nanoscale α-type silicon carbide as the main raw material, introducing graphene and carbon nanotubes as the first sintering aid, introducing boron carbide as the second sintering aid, introducing polystyrene sulfonate as a water reducer, and introducing silicon micropowder And talcum powder as other additives. The weight percent composition of each component in the preparation method is as follows: the first sintering aid accounts for 7%, the second sintering aid accounts for 3%, the water reducing agent accounts for 1%, other additives account for 1%, and silicon carbide accounts for 88%. %. Graphene:carbon nanotubes=3:7 in the first sintering aid. Microsilica powder:talc powder=0.4:0.6 in other additives.
[0026] Prepare premixed slurry. Dissolving part of the water reducer in the prepared solution, adding s...
Embodiment 2
[0029] This embodiment proposes a method for preparing a silicon carbide ceramic sealing ring, which may include the following steps: preparing raw materials. Using nanoscale α-type silicon carbide as the main raw material, introducing graphene and carbon organic precursor (phenolic resin) as the first sintering aid, introducing boron carbide as the second sintering aid, and introducing polystyrene sulfonate as the reducing agent Aqueous agent, introducing silicon micropowder and talcum powder as other additives. The weight percent composition of each component in the preparation method is as follows: the first sintering aid accounts for 7%, the second sintering aid accounts for 3%, the water reducing agent accounts for 1%, other additives account for 1%, and silicon carbide accounts for 88%. %. Graphene:phenolic resin=3:7 in the first sintering aid. Microsilica powder:talc powder=0.4:0.6 in other additives.
[0030] Prepare premixed slurry. Dissolving part of the water re...
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