Tree sticker capable of being used for repairing wounds, filling gaps, slowly releasing medicines and reinforcing strength
A tree sticker and drug technology, applied in the field of chemical materials and plant wound healing and protection, can solve the problems of thin film, difficult to fix, fragile and easy to break the trunk, and aggravate the risk of tree death.
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[0120] The present invention also provides a preparation method of the gum, comprising the steps of:
[0121] (i) providing an aqueous solution of a divalent metal salt, an aqueous solution of polyvinyl alcohol, and optionally an aqueous solution of a drug;
[0122] (ii) mixing the above-mentioned solutions in proportion to obtain a mixed solution; and
[0123] (iii) freezing and thawing the mixed solution obtained in step (ii) at low temperature to obtain the gum.
[0124] In step (ii), there is no special requirement on the mixing order, and the mixing can be done simultaneously or sequentially.
[0125] Those skilled in the art should understand that it is convenient to mix the divalent metal salt, PVA, and medicine after they are made into solutions, but mixing in other forms is also included within the scope of the present invention.
[0126] In a preferred embodiment, the method includes the steps of stirring and dissolving the PVA solution in hot water at 60-100°C, mi...
Embodiment 1
[0158] Preparation of gum
[0159] The gum is prepared according to the formula in Table 1. If there is no special instruction, by weight, the gained gum finally includes:
[0160] Table 1
[0161] CaCl 2
PVA Drugs (CuSO 4 )
Deionized water control group - 15 - 75 Freeze at -20°C Experimental group 1 10 15 - 75 Freeze at -20°C Experimental group 2 10 15 0.1g / mL 75 Freeze at -20°C Experimental group 3 10 15 - 75 room temperature
[0162] Specifically, the preparation steps are as follows: prepare CaCl with deionized water respectively 2 Solution (mix well at room temperature), PVA solution (heat at 75-80°C for about one hour), copper (II) sulfate solution (mix well at room temperature);
[0163] Mix the above solutions;
[0164] The mixture was frozen at -20°C for 24 hours and then thawed.
[0165]The results showed that when no metal salt was added for modification, the PVA aqueous solution could ...
Embodiment 2
[0167] Peel strength test
[0168] The steps are as follows: the wood is placed horizontally, and the surface of the wood is smoothed with sandpaper;
[0169] Draw an area 320mm long and 50mm wide on both sides of the wood;
[0170] Spread the sample evenly within the marked area, and then paste a carbon fiber cloth with a length of 420mm and a width of 50mm in the marked area;
[0171] Flatten the sample under the carbon fiber cloth, and spread the spilled sample evenly on the carbon fiber cloth, wrap it in plastic wrap and flatten it again;
[0172] After each sample was prepared, it was left to cure for seven days, and then the sample was placed under the tensile machine for testing, and the carbon fiber cloth at the end of the wood was fixed with the MTS machine, and then the sample was peeled off in the displacement control mode;
[0173] Then start the tensile test at a loading speed of 0.5mm per minute until the carbon fiber cloth begins to be pulled away from the woo...
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