Deep ultraviolet LED with component gradient quantum well structure and preparation method
A composition gradient and quantum well technology, which is applied in nanotechnology, electrical components, nanotechnology, etc. for materials and surface science, can solve the problem of low efficiency of deep ultraviolet LEDs, and achieve an increase in the equivalent barrier height and increase Luminous efficiency, effect of promoting recombination
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[0023]For the second solution proposed by the present invention, the steps of the method for preparing a deep ultraviolet LED with a composition graded quantum well structure include:
[0024] (1) Growth of AlN intrinsic layer. In this step, the low-temperature buffer layer in the AlN intrinsic layer is grown on the sapphire substrate under the condition of 400-800°C, with a thickness of 10-50nm; An intrinsic layer of AlN is grown on the layer, and the total thickness of the intrinsic layer of AlN is 500-4000nm.
[0025] (2) An n-type AlGaN electron injection layer is grown. In this step, the temperature is lowered to 800-1200°C, and an n-type AlGaN electron injection layer is grown on the AlN intrinsic layer, wherein the Al composition percentage is 20-90%, the thickness is 500-4000nm, and Si is used as the n-type dopant .
[0026] (3) Growing quantum well active layers with gradually changing composition. In this step, under the condition of lowering the temperature to 7...
Embodiment 1
[0032] In this example, the steps for preparing a deep ultraviolet LED with a composition-graded quantum well structure are as follows:
[0033] (1) At 600°C, grow a low-temperature buffer layer in the AlN intrinsic layer on a sapphire substrate with a thickness of 12nm; raise the temperature to 1200°C, and grow an AlN intrinsic layer on the low-temperature buffer layer in the AlN intrinsic layer , the total thickness of the AlN intrinsic layer is 750 nm.
[0034] (2) The temperature is lowered to 900° C., and an n-type AlGaN electron injection layer is grown on the AlN intrinsic layer with a thickness of 1200 nm.
[0035] (3) Lower the temperature to 800°C, and grow a quantum well active layer with a graded composition on the n-type AlGaN electron injection layer. The quantum well active layer with a graded composition includes an AlGaN barrier layer with a graded composition and a constant composition The AlGaN potential well layer, specifically, the AlGaN potential well la...
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