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Preparation device and method of magnesium hydroxide slurry

A technology of magnesium hydroxide and preparation device, applied in magnesium hydroxide, chemical instruments and methods, chemical/physical processes, etc., can solve the problems of difficulty in preparing high-concentration slurry, low hydration rate, long hydration time, etc. , to achieve the effect of automatic control, small solid particle size and difficult precipitation

Pending Publication Date: 2021-03-09
辽宁荣邦科技有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The hydration rate of the usual magnesium oxide hydration to prepare magnesium hydroxide process is not high, the hydration time is long, and the slurry is easy to precipitate after being placed for a long time, so it is difficult to prepare a stable high-concentration slurry

Method used

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  • Preparation device and method of magnesium hydroxide slurry
  • Preparation device and method of magnesium hydroxide slurry
  • Preparation device and method of magnesium hydroxide slurry

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] Such as Figure 1-2 As shown, a preparation device for magnesium hydroxide slurry includes a mixing tank 1, a hydrator 2 and a storage tank 3 connected in sequence, the mixing tank 1 is used for containing and mixing raw materials, and the hydrator 2 is a material The main reaction place, the storage tank 3 is used to collect the prepared magnesium hydroxide slurry. The hydrator 2 includes a feed port 5, a driving device 6, a reducer 7, an agitator shaft 8, an air pressure control valve 9, a baffle 10, a controller 11 and a discharge port 12, and the feed port 5 of the hydrator 2 passes through The pipeline is connected with the mixing tank 1 , and the discharge port 12 is connected with the storage tank 3 . The driving device 6 is a motor, the output end of the motor is connected with the reducer 7, the output end of the reducer 7 is connected with the stirring shaft 8, and the stirring shaft 8 extends into the inside of the hydrator 2, and the hydration reaction is p...

Embodiment 2

[0037] Such as image 3 As shown, the difference from Example 1 is that a preparation device for magnesium hydroxide slurry includes two hydrators 2, and the two hydrators 2 are connected in series. Specifically, the mixed material passes through the first hydrator 2 and the second hydrator 2 sequentially along the conveying direction, and the two-stage hydration makes the hydration reaction more complete.

[0038] A kind of preparation method based on the high concentration magnesium hydroxide slurry of above-mentioned device, comprises the steps:

[0039] (1) Add 1000-mesh light-burned magnesia powder, tap water, seawater and monosaccharide dispersant into the mixing tank 1, and mix evenly to obtain a slurry. The mass ratio of tap water to seawater is 1:10, the mass fraction of light-burned magnesia in the slurry is 27%, and the mass fraction of monosaccharide dispersant in the slurry is 1%.

[0040] (2) The slurry obtained in step (1) is fed into the first hydrator 2 thro...

Embodiment 3

[0046] The difference with embodiment 2 is that a kind of preparation method of magnesium hydroxide slurry comprises the steps:

[0047] (1) Add 3000-mesh light-burned magnesia powder, tap water, salt lake brine and monosaccharide dispersant into the mixing tank 1, and mix evenly to obtain a slurry. The mass ratio of tap water to salt lake brine is 1:15, the mass fraction of light-burned magnesia in the slurry is 60%, and the mass fraction of monosaccharide dispersant in the slurry is 5%.

[0048] (2) The slurry obtained in step (1) is fed into the first hydrator 2 through a peristaltic pump and a feed port 5 . At the same time, turn on the rotating motor to drive the stirring shaft 8 and the stirring paddle 14 to rotate at a speed of 500 rpm, propel and stir the mixed slurry, and promote the hydration of the magnesium oxide powder to form the magnesium hydroxide slurry.

[0049] (3) When the volume of the slurry reaches 2 / 3-3 / 4 of the volume of the first hydrator 2, stop fee...

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Abstract

The invention discloses apreparation device and method of a magnesium hydroxide slurry. The preparation device comprises a mixing tank, a storage tank and at least one hydrator; the hydrator comprisesa feeding port, a driving device, a speed reducer, a stirring shaft, an air pressure control valve, a baffle, a controller and a discharging port, wherein the feeding port is connected with the mixing tank, the discharging port is connected with the storage tank, the stirring shaft is connected with the driving device, the driving device is connected with the speed reducer, the output end of thespeed reducer is connected with the stirring shaft, and the stirring shaft extends into the hydrator; the hydrator is provided with the air pressure control valve capable of regulating and controllingthe internal pressure of the hydrator, the baffle is arranged at the discharging port, the controller is arranged outside the hydrator, and the controller controls the baffle; the invention further discloses a magnesium hydroxide slurry preparation method based on the device. Magnesium-containing water is used as a hydrating agent and process water, so that the dissolution rate of magnesium oxidecan be increased; meanwhile, a magnesium source is added, high-speed shearing and stirring are adopted, so that the hydration rate of the magnesium hydroxide is greatly increased, and stable high-concentration magnesium hydroxide slurry can be rapidly prepared.

Description

technical field [0001] The invention belongs to the technical field of chemical slurry preparation, and in particular relates to a preparation device and method of magnesium hydroxide slurry. Background technique [0002] Magnesium hydroxide has been widely studied in recent years because of its high activity, high adsorption capacity, strong buffer performance, safe use and low corrosion, and many other unique properties, as well as its abundant raw material reserves. The methods for obtaining magnesium hydroxide slurry in industry usually include magnesium oxide hydration method, brine precipitation method, brucite wet pulverization method, etc. The brine precipitation method has problems such as low purity and high cost; the brucite method wet crushing method is relatively simple, but the ore has a small content in nature; currently the most widely used method is the magnesia hydration method. The ore is the main raw material, which is calcined to make active magnesium o...

Claims

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Application Information

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IPC IPC(8): B01J19/20C01F5/14
CPCB01J19/20B01J19/0066C01F5/14B01J2219/00058
Inventor 王宁会孙守刚孟庆臻朱益民刘伟凤唐晓佳闯恒超杜钟原
Owner 辽宁荣邦科技有限公司