Preparation method of ecological functional leather based on nano material
An ecological function and nano-material technology, applied in leather impregnation, leather surface treatment, small raw hide/big raw hide/leather/fur treatment, etc., to achieve the effect of improving softness, improving wear resistance and reducing dosage
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Embodiment 1
[0053] A method for preparing ecologically functional leather based on nanomaterials, comprising the steps of:
[0054] Step 1: Preparation of nano-titanium dioxide-polyurethane retanning agent
[0055] (1) Take 5 parts of nano-titanium dioxide in a reaction vessel, add 0.4 parts of aminosilane coupling agent, 0.1 part of epoxy silane coupling agent, 50 parts of water, 100 parts of ethanol, stir and disperse, adjust pH = 10, and then ultrasonic Disperse for 5 minutes, react at a temperature of 30°C for 5 hours, filter, wash, and dry to obtain modified nano-titanium dioxide;
[0056] (2) Take 3 parts of polytetramethylene glycol, add to the reactor after dehydration treatment, add 0.8 parts of isophorone diisocyanate, and pre-polymerize at 80°C for 2 hours. Cool down to 65°C, add 0.4 parts of acetone to dilute, add 0.3 parts of butanediol, and react for 4 hours. Add 0.1 part of dimethylolpropionic acid, react for 2h. Cool down to 50°C, add 0.1 part of triethylamine to neutra...
Embodiment 2
[0101] A method for preparing ecologically functional leather based on nanomaterials, comprising the steps of:
[0102] The method of present embodiment 2 is identical with embodiment 1, difference is anion filling process, anion filling dyeing process, specifically as follows:
[0103] (5) Anion filling: Add 50% water and 3% nano-titanium dioxide-polyurethane retanning agent to the drum, control the temperature to 30°C, and rotate for 10 minutes. Add 2% acrylic resin retanning agent TP340 (ALPA Leather Chemical Company), 3% acrylic resin retanning agent CC (Xiamen Wantongli Chemical Materials Co., Ltd.), and rotate for 60 minutes. Add 0.5% anionic fatliquoring agent OSL (Toppler), 2% synthetic tanning agent FO (BASF), 3% amino resin tanning agent HB (Toppler), 2% protein filler FB (Desaier Chemical Industry Co., Ltd.), rotate for 90 minutes. Add 100% water, add 1% formic acid, control the temperature at 30°C, rotate for 20min, add 1% formic acid, rotate for 20min.
[0104]...
Embodiment 3
[0106] A method for preparing ecologically functional leather based on nanomaterials, comprising the steps of:
[0107] The method of present embodiment 3 is identical with embodiment 1, difference is anion filling process, anion filling dyeing process, specifically as follows:
[0108] (5) Anion filling: add 50% water into the drum, add 2% nanometer titanium dioxide-polyurethane retanning agent, control the temperature at 30°C, and rotate for 10 minutes. Add 2% acrylic resin retanning agent TP340 (ALPA Leather Chemical Company), 3% acrylic resin retanning agent CC (Xiamen Wantongli Chemical Materials Co., Ltd.), and rotate for 60 minutes. Add 0.5% anionic fatliquoring agent OSL (Toppler), 2% synthetic tanning agent FO (BASF), 3% amino resin tanning agent HB (Toppler), 2% protein filler FB (Desaier Chemical Industry Co., Ltd.), rotate for 90 minutes. Add 100% water, add 1% formic acid, control the temperature at 30°C, rotate for 20min, add 1% formic acid, rotate for 20min. ...
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