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A kind of preparation technology of tin-lead alloy material with low melting point and high pressure resistance

A tin-lead alloy and preparation process technology, which is applied in the field of metal material design to achieve the effects of high compressive strength, low production cost and equipment safety protection

Active Publication Date: 2022-03-29
ZHEJIANG COLLEGE OF ZHEJIANG UNIV OF TECHOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Although vehicle-mounted high-pressure gaseous hydrogen storage technology has been widely used, there are still many technical bottlenecks in my country's high-performance vehicle-mounted high-pressure hydrogen storage system

Method used

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  • A kind of preparation technology of tin-lead alloy material with low melting point and high pressure resistance
  • A kind of preparation technology of tin-lead alloy material with low melting point and high pressure resistance
  • A kind of preparation technology of tin-lead alloy material with low melting point and high pressure resistance

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Experimental program
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Effect test

Embodiment 1

[0035] A preparation process of a low-melting-point high-pressure-resistant tin-lead alloy material of the present embodiment comprises the following steps:

[0036] (1) Prepare raw materials according to the following parts by mass: 1 part of tin, 30 parts of lead, 40 parts of bismuth, and 0.005 part of cadmium; wherein the purity of tin is ≥99.8%, the purity of lead is ≥99.8%, and the purity of bismuth is ≥99.8%. The tin material, lead material and bismuth material are lumpy with a size of 22mm, and the cadmium material is spherical with a diameter of 5mm.

[0037] (2) Put the above-mentioned raw materials of lead, bismuth and cadmium into the smelting furnace, adjust the smelting temperature to 700°C for smelting, and stir and melt;

[0038] (3) Adjust the smelting temperature to 300°C. When the temperature in the furnace drops to 300°C, add the above-mentioned tin raw material by mass, stir until it is completely melted, remove the surface slag, and let it stand to obtain ...

Embodiment 2

[0044] A preparation process of a low-melting-point high-pressure-resistant tin-lead alloy material of the present embodiment comprises the following steps:

[0045] (1) Prepare raw materials according to the following mass parts: 35 parts of tin, 40 parts of lead, 50 parts of bismuth, and 0.015 parts of cadmium; wherein the purity of tin is ≥99.8%, the purity of lead is ≥99.8%, and the purity of bismuth is ≥99.8%. Tin material, lead material and bismuth material are in block shape with a size of 28mm, and cadmium material is in block shape with a diameter of 5mm.

[0046] (2) Put the above-mentioned raw materials of lead, bismuth and cadmium into the smelting furnace, adjust the smelting temperature to 750°C for smelting, and stir and melt;

[0047](3) Adjust the smelting temperature to 330°C. When the temperature in the furnace drops to 330°C, add the above-mentioned tin raw material by mass, stir until it is completely melted, remove the slag from the surface layer, and let...

Embodiment 3

[0053] A preparation process of a low-melting-point high-pressure-resistant tin-lead alloy material of the present embodiment comprises the following steps:

[0054] (1) Prepare raw materials according to the following parts by mass: 5 parts of tin, 45 parts of lead, 60 parts of bismuth, and 0.025 parts of cadmium; wherein the purity of tin is ≥99.8%, the purity of lead is ≥99.8%, and the purity of bismuth is ≥99.8%. Tin material, lead material and bismuth material are lumpy with a size of 40mm, and cadmium material is spherical with a diameter of 6mm.

[0055] (2) Put the above-mentioned lead, bismuth, and cadmium raw materials in the melting furnace, adjust the melting temperature to 800°C for refining, and stir and melt;

[0056] (3) Adjust the smelting temperature to 350°C. When the temperature in the furnace drops to 350°C, add the above-mentioned tin raw material by mass, stir until it is completely melted, remove the surface slag, and let it stand to obtain an alloy hot...

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Abstract

The invention provides a preparation process of a low-melting-point high-pressure-resistant tin-lead alloy material, relates to the technical field of metal material design, and includes material preparation: raw material preparation according to the following parts by mass: 1-15 parts of tin, 30-45 parts of lead, bismuth 40-60 parts, 0.005-0.025 parts of cadmium; put the tin, lead, and cadmium raw materials into the melting furnace, adjust the melting temperature to 700-800°C for refining, and stir and melt; adjust the melting temperature to 300-350 ℃, add tin raw material, stir until it is completely melted, remove the surface slag, and let it stand still to obtain a metal hot melt; filter the mixed hot melt, put it into a mold, and obtain a metal ingot after cooling; Ingots are processed into metal cylinders; cleaned and shaped; packaged and put into storage. The invention has simple process, the whole process can be carried out in the atmospheric environment, the production cost is low, the operation is easy, and it is suitable for widespread use. The alloy has a low melting point and a small melting range, and can work under the condition of 70MPa high-pressure hydrogen.

Description

technical field [0001] The invention relates to a preparation process of a low melting point and high pressure resistant tin-lead alloy material, which belongs to the technical field of metal material design. Background technique [0002] Compared with traditional fossil energy such as petroleum and coal, hydrogen energy has the advantages of being clean and environmentally friendly, diverse sources, and scalable storage and transportation, and plays an important role in the energy structure. As an energy storage component of hydrogen fuel cell vehicles, convenient and efficient storage of hydrogen is one of the key technologies to realize the large-scale commercialization of hydrogen fuel cell vehicles. High-pressure gaseous hydrogen storage and liquid hydrogen storage are two main hydrogen storage methods, which have been popularized and applied. High-pressure gaseous hydrogen storage has the advantages of simple container structure, less energy consumption for compressed...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C12/00C22C30/04C22C1/02
CPCC22C12/00C22C30/04C22C1/02
Inventor 骆芳沈逸周蒋荣杰路远航柴为民袁林江
Owner ZHEJIANG COLLEGE OF ZHEJIANG UNIV OF TECHOLOGY