A thermal radiator with a three-dimensional core-shell opal structure for thermal photovoltaics and its preparation method
A heat radiator and core-shell protein technology, which is applied in the field of three-dimensional core-shell opal structure heat radiators for thermal photovoltaics and its preparation, can solve the problems of low spectral efficiency, high manufacturing cost and high cost of photonic crystal heat radiators, etc.
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Embodiment 1
[0233] This embodiment provides a heat radiator with a three-dimensional core-shell opal structure, and its preparation method is as follows:
[0234] 1) Take 0.5g of metal tungsten powder with a particle size of 50nm, and disperse it in 100ml of absolute ethanol for ultrasonic dispersion (the frequency of ultrasonic dispersion is 25kHz and the temperature is 25°C) for 20min to obtain a metal tungsten nanoparticle dispersion (tungsten nanoparticle The number density of the particles is 3.9×10 12 pieces / ml).
[0235] 2) Add 0.3ml of 3-aminopropyltriethoxysilane (APS) to the above-mentioned metal tungsten nanoparticle dispersion liquid, then ultrasonically disperse (the frequency of ultrasonic dispersion is 25kHz and the temperature is 25°C) for 5min, and transfer it into 250ml in a round-bottomed flask at 30°C with magnetic stirring at 800rpm, and stop stirring after 24 hours. This step is to modify the APS macromolecular chains on the outer surface of tungsten nanoparticles t...
Embodiment 2
[0246] This embodiment provides a heat radiator with a three-dimensional core-shell opal structure, the preparation method of which is the same as that of Embodiment 1, the difference is that in step 1), the particle size of metal tungsten powder is measured to be 100 nm.
[0247] Effect
[0248] The scanning electron microscope (SEM) picture of the silica@tungsten core-shell nanospheres prepared in Example 2 is as follows Figure 5 As shown, it can be seen that the particle size of the prepared silica@metal core-shell nanospheres is about 510nm, and it can be seen from the light and dark parts of the particles that they are composed of core-shell structures.
Embodiment 3
[0250] This embodiment provides a heat radiator with a three-dimensional core-shell opal structure. Its preparation method is the same as that of Embodiment 1, except that the amount of ammonia water added in step 5) is 1 ml, and the amount of ultrapure water added is 3 ml.
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