Preparation and production process of high-purity magnesium oxide
A production process and technology of magnesium oxide, applied in directions such as magnesium oxide, can solve the problems of difficult to control reaction conditions, high cost, insufficient purity of magnesium oxide, etc., and achieve the effects of easy control of process parameters, reduction of impurity content, and low production cost.
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Embodiment 1
[0032] (1) Measure 246kg of magnesium sulfate heptahydrate, place the magnesium sulfate heptahydrate in a ventilated crucible with a top cover structure, put the crucible in a drying kiln, control the temperature of the drying kiln at 350°C, and dry it through the drying kiln After 4 hours, take out to obtain dry anhydrous magnesium sulfate, and dry the water to discharge;
[0033] (2) Anhydrous magnesium sulfate is transported in the mill, and through sufficient grinding, the particle size is controlled at 200 orders;
[0034] (3) Add 15kg of active carbon into the ground anhydrous magnesium sulfate, and after fully mixing anhydrous magnesium sulfate and active carbon, send it into the roller kiln for high-temperature calcination. The calcination temperature is 1100° C., and the calcination time is 5h, discharge sulfur dioxide;
[0035] (4) Add 80L of primary washing water into the primary washing tank, control the temperature at 50°C, put the calcined magnesium oxide into t...
Embodiment 2
[0040] (1) Measure 600kg of magnesium sulfate heptahydrate, place the magnesium sulfate heptahydrate in a ventilated crucible with a top cover structure, put the crucible in a drying kiln, control the temperature of the drying kiln at 350°C, and dry it in the drying kiln Take out after 3h to obtain dry anhydrous magnesium sulfate, and dry the water to discharge;
[0041] (2) Anhydrous magnesium sulfate is transported in the mill, and through sufficient grinding, the particle size is controlled at 250 orders;
[0042] (3) Add 37kg of active carbon into the ground anhydrous magnesium sulfate, and after fully mixing anhydrous magnesium sulfate and active carbon, send it into the roller kiln for high-temperature calcination. The calcination temperature is 1150° C., and the calcination time is 4h, discharge sulfur dioxide;
[0043] (4) Add 195L of primary washing water into the primary washing tank, control the temperature at 70°C, put the calcined magnesium oxide into the primary...
Embodiment 3
[0048] (1) Measure 100kg of magnesium sulfate heptahydrate, place the magnesium sulfate heptahydrate in a ventilated crucible with a top cover structure, put the crucible in a drying kiln, control the temperature of the drying kiln at 250°C, and dry it through the drying kiln Take out after 2h to obtain dry anhydrous magnesium sulfate, and dry the water to discharge;
[0049] (2) Anhydrous magnesium sulfate is transported in the mill, and through sufficient grinding, the particle size is controlled at 300 mesh;
[0050] (3) Add the gac of 6kg in the anhydrous magnesium sulfate after grinding, after fully mixing anhydrous magnesium sulfate and gac mix, send into the roller kiln and carry out high-temperature calcination, and the calcination temperature is 950 ℃, and the calcination time is 3.5h, sulfur dioxide discharge;
[0051] (4) Add 32.5L of primary washing water into the primary washing tank, control the temperature at 40°C, put the calcined magnesium oxide into the prim...
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