High-strength creep-resistant polyester industrial yarn and preparation method thereof
A technology of polyester industrial yarn and creep resistance, applied in the field of spinning, can solve problems such as traffic accidents, elongation and deformation of tire frame, etc., and achieve the effects of reducing creep degree, increasing elastic modulus, and good mechanical properties
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[0053]Example 1
[0054]Method for preparing high-strength creep polyester industrial filaments, specific steps are as follows:
[0055](1) Preparation of modified polyester;
[0056](1.1) esterification reaction;
[0057]Tobenipateic acid, ethylene glycol, and 2- (4-pyridine) of 1: 1.2: 0.03 were used as a slurry, add catalyst (trioxide) and stabilizer (triphenyl phosphate). The addition of mixing is uniform, the amount of the catalyst and the stabilizer is 0.01% by weight and 0.03% by weight of terephthalic acid added, and then the esterification reaction is performed in a nitrogen atmosphere, and the pressure pressure is 0.2 MPa, esterification reaction. The temperature is 259 ° C, and when the amount of the die in the esterification reaction reaches 96% of the theoretical value, it is the endpoint of esterification reaction;
[0058](1.2) polycondensation reaction;
[0059]After the esterification reaction, the polycondensation reaction of the low vacuum stage was started under negative pressure ...
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[0075]Example 2
[0076]Method for preparing high-strength creep polyester industrial filaments, specific steps are as follows:
[0077](1) Preparation of modified polyester;
[0078](1.1) esterification reaction;
[0079]Tobenylene terephthalic acid, ethylene glycol, and 2- (4-pyridine) of 1: 1.5: 0.03 were used as a slurry, add catalyst (trioxide) and stabilizer (triphenyl phosphate). The addition of mixed uniform, the amount of the catalyst and the stabilizer is 0.01% by weight and 0.04% by weight of terephthalic acid added, and then the esterification reaction is performed in a nitrogen atmosphere, and the pressure pressure is 0.2 MPa, esterification reaction. The temperature is 260 ° C, and the end of the esterification reaction when the reflection in the esterification reaction reaches 96% of the theoretical value;
[0080](1.2) polycondensation reaction;
[0081]After the esterification reaction, the polycondensation reaction of the low vacuum stage was started under negative pressure conditio...
Example Embodiment
[0097]Example 3
[0098]Method for preparing high-strength creep polyester industrial filaments, specific steps are as follows:
[0099](1) Preparation of modified polyester;
[0100](1.1) esterification reaction;
[0101]Benzothylene terephthalic acid, ethylene glycol, and 2- (4-pyridine) of 1: 2.0: 0.03 were used as a slurry, add catalyst (trioxide) and stabilizer (trimethylate phosphate). The addition of mixing, the addition of the catalyst and the stabilizer is 0.02% and 0.05 wt% of terephthalic acid added, and then the esterification reaction is performed in a nitrogen atmosphere, and the pressure pressure is 0.3 MPa, esterification reaction. The temperature is 254 ° C, and the end point of the esterification reaction when the amount of the reflection in the esterification reaction reaches 95% of the theoretical value;
[0102](1.2) polycondensation reaction;
[0103]After the esterification reaction, the polycondensation reaction of the low vacuum stage was started under negative pressure condi...
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