Antibacterial moisturizing degradable porous gel preservative film and preparation method thereof
A fresh-keeping film and gel technology, applied in the field of antibacterial, moisturizing and degradable porous gel fresh-keeping film and its preparation, can solve the problems of narrow bacteriostatic range, poor mechanical strength and the like
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Embodiment 1
[0033] (1) Preparation of component A solution: Weigh 60 parts of methacrylic acid monomer and put it in 100 parts of deionized water, stir and dissolve, add 30 parts of double-long-chain methyl tertiary amine and 1 part of cuprous bromide in sequence, and store at 22 °C Under the condition of stirring and reacting for 20min, A component solution was obtained;
[0034] (2) Preparation of component B solution: Weigh 20 parts of ferulic acid, put it in 60 parts of ethanol solution, stir and disperse, add 15 parts of 3,4-ethylenedioxythiophene, and stir and react at 22°C for 60 minutes to obtain B component solution;
[0035](3) Synthetic fresh-keeping slurry: 40 parts of chitosan are placed in 50 parts of acetic acid solution and stirred and dissolved, while stirring, 45 parts of component A solution and 25 parts of component B solution are added to the chitosan solution, adding After finishing, add 10 parts of chloroethanol with the addition rate of V1, obtain the preservative...
Embodiment 2
[0043] (1) Preparation of component A solution: Weigh 75 parts of methacrylic acid monomer and put it in 110 parts of deionized water, stir and dissolve, add 34 parts of double-long-chain methyl tertiary amine and 2 parts of cuprous bromide in sequence, and store at 24 °C Under the condition of stirring and reacting for 23min, the solution of component A was obtained;
[0044] (2) Preparation of component B solution: Weigh 25 parts of ferulic acid and place it in 65 parts of ethanol solution to stir and disperse, add 18 parts of 3,4-ethylenedioxythiophene, and stir and react at 25°C for 65 minutes to obtain B component solution;
[0045] (3) Synthesis of fresh-keeping slurry: 43 parts of chitosan are placed in 53 parts of acetic acid solution and stirred and dissolved, while stirring, 48 parts of component A solution and 28 parts of component B solution are added to the chitosan solution, adding After finishing, add 11 parts of chloroethanol with the addition rate of V1, obta...
Embodiment 3
[0053] (1) Preparation of component A solution: Weigh 90 parts of methacrylic acid monomer and put it in 110 parts of deionized water, stir and dissolve, add 36 parts of double long-chain methyl tertiary amine and 2 parts of cuprous bromide in sequence, Under the condition of stirring and reacting for 26 minutes, the solution of component A was obtained;
[0054] (2) Preparation of component B solution: Weigh 30 parts of ferulic acid, put it in 72 parts of ethanol solution, stir and disperse, add 23 parts of 3,4-ethylenedioxythiophene, and stir and react at 25°C for 72 minutes to obtain B component solution;
[0055] (3) Synthesis of fresh-keeping slurry: 46 parts of chitosan are placed in 56 parts of acetic acid solution and stirred and dissolved, while stirring, 52 parts of component A solution and 32 parts of component B solution are added to the chitosan solution, adding After finishing, add 13 parts of chloroethanol with the addition speed of V1, obtain the preservative ...
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