Flame-retardant antibacterial high-performance garment fabric and preparation method thereof
A high-performance, clothing technology, applied in the manufacture of fire-retardant and flame-retardant filaments, rayon, and textiles. Product with good aesthetics
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Embodiment 1
[0025] Take Si(NO 3 ) 2 After preliminary grinding, it was dissolved in absolute ethanol solution according to 1:10, magnetically stirred for 3 hours to form a transparent solution, and then triethanolamine was slowly added dropwise to the solution to adjust the pH value of the solution to 6 to form a coagulated colloid; The colloid was placed in an oven at 80° C. and dried for 15 hours, then the powder was taken out, ground, and heat treated at 400° C. for 2 hours to obtain nano-Si(NO 3 ) 2 powder; after the powder is dispersed in concentrated sulfuric acid, after 110 ° C high-temperature treatment, modified nano-Si (NO 3 ) 2 powder, for later use; add terephthalic acid and dimethylformamide into the reaction vessel, stir and dissolve, add thionyl chloride therein, heat up to 80°C for reflux reaction for 4h, and then carry out vacuum distillation to obtain terephthalic di formyl chloride; dissolve terephthaloyl chloride in acetone, then add 2,4-diaminophenol therein, heat...
Embodiment 2
[0027] Take Si(NO 3 ) 2 After preliminary grinding, it was dissolved in absolute ethanol solution according to 1:10, magnetically stirred for 3 hours to form a transparent solution, and then triethanolamine was slowly added dropwise to the solution to adjust the pH value of the solution to 6 to form a coagulated colloid; The colloid was placed in an oven at 80° C. and dried for 15 hours, then the powder was taken out, ground, and heat treated at 400° C. for 2 hours to obtain nano-Si(NO 3 ) 2 powder; after the powder is dispersed in concentrated sulfuric acid, after 110 ° C high-temperature treatment, modified nano-Si (NO 3 ) 2powder, for later use; add terephthalic acid and dimethylformamide into the reaction vessel, stir and dissolve, add thionyl chloride therein, heat up to 80°C for reflux reaction for 4h, and then carry out vacuum distillation to obtain terephthalic di formyl chloride; dissolve terephthaloyl chloride in acetone, then add 2,4-diaminophenol therein, heat ...
Embodiment 3
[0029] Take Si(NO 3 ) 2 After preliminary grinding, it was dissolved in absolute ethanol solution according to 1:10, magnetically stirred for 3 hours to form a transparent solution, and then triethanolamine was slowly added dropwise to the solution to adjust the pH value of the solution to 6 to form a coagulated colloid; The colloid was placed in an oven at 80° C. and dried for 15 hours, then the powder was taken out, ground, and heat treated at 400° C. for 2 hours to obtain nano-Si(NO 3 ) 2 powder; after the powder is dispersed in concentrated sulfuric acid, after 110 ° C high-temperature treatment, modified nano-Si (NO 3 ) 2 powder, for later use; add terephthalic acid and dimethylformamide into the reaction vessel, stir and dissolve, add thionyl chloride therein, heat up to 80°C for reflux reaction for 4h, and then carry out vacuum distillation to obtain terephthalic di formyl chloride; dissolve terephthaloyl chloride in acetone, then add 2,4-diaminophenol therein, heat...
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