A kind of manufacturing method of high strength and high dimensional stability hmls polyester industrial yarn

A technology of dimensional stability and manufacturing method, applied in textile/flexible product manufacturing, single-component polyester rayon, final product manufacturing, etc., can solve the problem of poor dimensional stability, low strength, increased dry heat shrinkage, etc. problem, to achieve the effect of high dimensional stability, high fracture strength and high crystallinity

Active Publication Date: 2022-06-07
JIANGSU TAIJI IND NEW MATERIALS CO LTD
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] As we all know, under the same melt conditions, when producing high-strength HMLS polyester industrial yarn, compared with conventional HMLS polyester industrial yarn and HMLS polyester industrial yarn with high dimensional stability, the draft ratio needs to be larger, within a certain range As the post-drawing ratio increases, the strength of the original yarn increases, the dry heat shrinkage increases, the elongation at constant load decreases, and the dimensional stability of the original yarn decreases.
In the production of HMLS polyester industrial yarn with high dimensional stability, under the same melt conditions, the subsequent draft ratio is equivalent to that of conventional polyester industrial yarn, but smaller than that of high-strength polyester HMLS industrial yarn, and its original filament size The stability is much better than high tenacity HMLS polyester industrial yarn, but its strength is far less than high tenacity HMLS polyester industrial yarn
High-strength HMLS polyester industrial yarn needs to prepare high-viscosity polyester chips, high oil-free silk viscosity and high draw ratio to obtain high-strength HMLS polyester industrial yarn. In the actual production process, under this condition The production stability of industrial yarns is generally poor, which brings a load to production stability. At the same time, the dimensional stability of the high-strength HMLS polyester industrial yarns produced is worse than that of conventional polyester HMLS industrial yarns.
[0005] The manufacture of HMLS polyester industrial yarn with high dimensional stability needs to increase the spinning speed, thereby increasing the spinning tension, increasing the degree of orientation and crystallinity of the as-drawn yarn, and the increase in spinning speed will bring about the loss of the strength of the original yarn, and its production The strength of the high dimensional stability HMLS polyester industrial yarn obtained is slightly lower than that of conventional HMLS polyester industrial yarn

Method used

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  • A kind of manufacturing method of high strength and high dimensional stability hmls polyester industrial yarn
  • A kind of manufacturing method of high strength and high dimensional stability hmls polyester industrial yarn
  • A kind of manufacturing method of high strength and high dimensional stability hmls polyester industrial yarn

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Effect test

Embodiment 1

[0023] A manufacturing method of high strength and high dimensional stability HMLS polyester industrial yarn, the specific production process comprises the following steps:

[0024] (1) Production of high-viscosity polyester chips: take low-viscosity polyester chips with a relative viscosity of 0.670 dl / g, carry out pre-crystallization of the low-viscosity polyester chips, the pre-crystallization temperature is 170 ° C, the pre-crystallization time is 20 min, and then Carry out solid-phase polycondensation and thickening at 210℃, the relative viscosity of polyester chips after thickening is 1.16dl / g, the water content is 27ppm, and the carboxyl group content is 9mol / t;

[0025] (2) Melt spinning process: the high viscosity polyester chips after solid phase polycondensation and thickening are fed into a 175mm screw extruder, heated and melted at 298 ° C to obtain a high viscosity polyester melt, and the melt is distributed through the main pipe Go to each melt branch pipe, and ...

Embodiment 2

[0031] A manufacturing method of high strength and high dimensional stability HMLS polyester industrial yarn, the specific production process comprises the following steps:

[0032] (1) Production of high-viscosity polyester chips: take low-viscosity polyester chips with a relative viscosity of 0.675, pre-crystallize the polyester chips, the pre-crystallization temperature is 185 ° C, the pre-crystallization time is 20 min, and then carried out at 220 ° C. Solid-phase polycondensation to increase viscosity, the relative viscosity of the slices after thickening is 1.21dl / g, the moisture content is 25ppm, and the carboxyl group content is 11mol / t;

[0033](2) Melt spinning process: the high-viscosity polyester chips obtained by solid-phase polymerization are fed into a 175mm screw extruder, heated and melted at 320 ° C to obtain a high-viscosity polyester melt, and the melt is distributed to each melt through the main pipe. The body branch pipe, and then enters the spinning asse...

Embodiment 3

[0040] A manufacturing method of high strength and high dimensional stability HMLS polyester industrial yarn, the specific production process comprises the following steps:

[0041] (1) Manufacture of high-viscosity polyester chips: take low-viscosity polyester chips with a relative viscosity of 0.675, and pre-crystallize the polyester chips. The solid-phase polycondensation increases the viscosity, so that the relative viscosity of the slices after solid-phase polymerization reaches 1.26dl / g, the water content is 24ppm, and the carboxyl group content is 12mol / t;

[0042] (2) Melt spinning process: the high-viscosity polyester chips obtained by solid-phase polymerization are fed into a 175mm screw extruder, heated and melted at 260 ° C to obtain a high-viscosity polyester melt, and the melt is distributed to each The melt branch pipe enters the spinning assembly through the metering pump. The melt main pipe, branch pipe, metering pump and components are heated and insulated wi...

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Abstract

The invention belongs to the technical field of polyester industrial yarn manufacturing, and in particular relates to a manufacturing method of high-strength and high-dimensional-stability HMLS polyester industrial yarn. In the present invention, conventional polyester chips are subjected to solid-phase polycondensation to form high-viscosity polyester chips, and then the high-viscosity polyester chips are passed through a spinning screw extruder to obtain a high-viscosity polyester melt, which is distributed to each melt through a melt main pipe. Body branch pipe, then enters the spinning assembly through the metering pump and extrudes from the spinneret of the assembly, heated by the heating cylinder, enters the blowing cooling, and then passes through the spinning tunnel; oils the surface of the silk, stretches at room temperature in the first stage, and stretches in the second stage Heat stretching, heat setting at high temperature and constant speed, and finally relaxation and setting, coiling and forming, the total stretching ratio is 1.75-2.20; and winding at 6400-7000 m / min, the polyester industrial yarn produced is strong It is 8.2‑8.5cN / dtex, and the dimensional stability is less than 8.0%. It can be widely used in the fields of light truck and car radial tires, V-belt hard cords, transmission belts, high-grade geogrids, high-end automobile tires, conveyor belts, hose tapes, etc. .

Description

technical field [0001] The invention belongs to the technical field of polyester industrial yarn manufacturing, and in particular relates to a manufacturing method of HMLS polyester industrial yarn with high strength and high dimensional stability. Background technique [0002] Since the development of polyester industrial yarn cords in the early 1960s, after years of development and improvement, the production technology, equipment and applications of polyester industrial yarns have become more and more mature. Due to the good performance of polyester industrial yarn, lower production cost and better production environment, it has become the four major rubber skeleton materials together with nylon, steel wire and viscose strong yarn; polyester industrial yarn is mainly used as rubber skeleton material , the driving force for its development first comes from the demand for tire radial development. [0003] With the development of high-grade highways and luxury cars, the spe...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01D5/12D01D1/00D01F6/62
CPCD01D5/12D01D1/00D01F6/62Y02P70/62
Inventor 许其军江晓峰刘全来陆福梅王晓龙
Owner JIANGSU TAIJI IND NEW MATERIALS CO LTD
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