Well cementation cement additive and use method thereof
A cementing cement and additive technology, applied in the field of oil field cementing, can solve problems such as low compressive strength and large water-solid ratio
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example 1
[0052] Step 1, mixing sodium alginate and water with a mass ratio of 1:10, adjusting the pH to 10 to obtain a mixed system;
[0053] Step 2. Add epichlorohydrin accounting for 5% of the mass of sodium alginate to the mixed system, react at 60° C. for 3.5 hours, add absolute ethanol, filter with suction, and dry to obtain cross-linked sodium alginate;
[0054] Step 3, dissolving the cross-linked sodium alginate in water, standing for defoaming, and preparing a 3% cross-linked sodium alginate solution by mass;
[0055] Step 4, the cross-linked sodium alginate solution is extruded into a calcium chloride solution with a mass percentage of 4% through a spinneret hole, the temperature of the coagulation bath is 40°C, and the average Cross-linked calcium alginate fibers with a diameter of 200 μm, the cross-linked calcium alginate fibers are cut to an average length of 0.5 mm;
[0056] Step 5. Mix cement and water evenly to make cement slurry, which will account for 10% of the cemen...
example 2
[0058] Step 1, mixing sodium alginate and water with a mass ratio of 1:10, adjusting the pH to 10 to obtain a mixed system;
[0059] Step 2. Add epichlorohydrin accounting for 5% of the mass of sodium alginate to the mixed system, react at 60° C. for 3.5 hours, add absolute ethanol, filter with suction, and dry to obtain cross-linked sodium alginate;
[0060] Step 3, dissolving the cross-linked sodium alginate in water, standing for defoaming, and preparing a 4% cross-linked sodium alginate solution by mass;
[0061] Step 4. The cross-linked sodium alginate solution is extruded into a calcium chloride solution with a mass percentage of 3% through a spinneret hole, and the temperature of the coagulation bath is 40° C. After traction, washing and drying, the average Cross-linked calcium alginate fibers with a diameter of 200 μm, the cross-linked calcium alginate fibers are cut to an average length of 0.5 mm;
[0062] Step 5, mix cement and water evenly to make cement slurry, ta...
example 3
[0065] Step 1, mixing sodium alginate and water with a mass ratio of 1:10, adjusting the pH to 10 to obtain a mixed system;
[0066] Step 2. Add epichlorohydrin accounting for 6% of the mass of sodium alginate to the mixed system, react at 60° C. for 3.5 hours, add absolute ethanol, filter with suction, and dry to obtain cross-linked sodium alginate;
[0067] Step 3, mixing cross-linked sodium alginate and sodium carboxymethyl cellulose in a molar ratio of 20:3 and dissolving in water, filtering and standing for defoaming to obtain a mixed spinning solution with a mass percentage of 5%;
[0068] Step 4, using 4% calcium chloride solution as the coagulation bath, extruding the mixed spinning solution into the coagulation bath through the spinneret hole, the temperature of the coagulation bath is 40°C, and then pulling, After washing and drying, cross-linked calcium alginate fibers with an average diameter of 200 μm were obtained, and the cross-linked calcium alginate fibers wer...
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