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Efficient and lasting antibacterial material and preparation method thereof

An antibacterial material and long-lasting technology, applied in the field of high-efficiency and durable antibacterial materials and their preparation, can solve the problems of weak binding between antibacterial materials and carbon fiber cloth, decreased antibacterial performance, and weak binding between antibacterial nanomaterials and inorganic carriers, etc.

Pending Publication Date: 2021-07-13
瑞安铭恩科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0006] Carbon fiber cloth is a commonly used material for clothing and insoles. The conventional addition of antibacterial materials is usually to directly coat a layer of antibacterial materials on its surface, or mix a part of antibacterial materials, but the combination of antibacterial materials and carbon fiber cloth is not firm. The number of times of use of clothing (the number of washings has the greatest impact) increases and the antibacterial performance decreases significantly. The main reason is that the combination of antibacterial nanomaterials and inorganic carriers is not firm. Therefore, it is necessary to develop a method that can enhance the combination of antibacterial nanomaterials and inorganic carriers The simple preparation process is particularly important

Method used

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  • Efficient and lasting antibacterial material and preparation method thereof
  • Efficient and lasting antibacterial material and preparation method thereof
  • Efficient and lasting antibacterial material and preparation method thereof

Examples

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Effect test

Embodiment 1

[0021] The preparation method of high-efficiency and durable antibacterial materials, the specific steps are as follows: a. Soak the bamboo charcoal fiber cloth in acetone, ethanol, and deionized water for 30 minutes respectively; then arrange the bamboo charcoal fiber in a constant temperature drying box and dry it at 60 ° C Standby; b. arrange the bamboo charcoal fiber under the dielectric barrier discharge equipment and process it for 30min, then put it into the thermal evaporation film cabin and fix it, put the Ag particles in the evaporation boat of the thermal evaporation film machine, and vacuum to 10 -3 Pa, set the current to control the evaporation rate as The time is 6min, and a layer of Ag nanoparticles is plated on the surface of the bamboo charcoal fiber cloth, with an average particle size of 4nm; c. 1mg polyvinylpyrrolidone, 10ml ethylene glycol and 0.1mg succinic acid are dissolved in 20ml deionized water in turn, and stirred for 60min , to form solution A, th...

Embodiment 2

[0023] The preparation method of high-efficiency and durable antibacterial materials, the specific steps are as follows: a. Soak the bamboo charcoal fiber cloth in acetone, ethanol, and deionized water for 30 minutes respectively; then arrange the bamboo charcoal fiber in a constant temperature drying box and dry it at 60 ° C Standby; b. arrange the bamboo charcoal fiber under the dielectric barrier discharge equipment and process it for 30min, then put it into the thermal evaporation film cabin and fix it, put the Ag particles in the evaporation boat of the thermal evaporation film machine, and vacuum to 10 -3 Pa, set the current to control the evaporation rate as The time is 6min, and the surface of the bamboo charcoal fiber cloth is plated with a layer of Ag nano crystal seeds, the average particle size is 4nm; c. 0.5mg polyvinylpyrrolidone, 5ml ethylene glycol and 0.05mg succinic acid are dissolved in 20ml deionized water successively, Stir for 60min to form solution A, th...

Embodiment 3

[0034] The difference between this embodiment and embodiment 2 is that the soaking ultrasonic time of step a is changed to 5, 60min, others are the same as embodiment 2, specifically as follows: a. the bamboo charcoal fiber cloth is placed in acetone, ethanol, deionized water successively to soak respectively Ultrasound for 5 and 60 minutes; then arrange the bamboo charcoal fibers in a constant temperature drying box, and dry them at 60°C for later use; b. Arrange the bamboo charcoal fibers under dielectric barrier discharge equipment for 30 minutes, and then put them into the thermal evaporation film cabin for fixation , put the Ag particles into the evaporation boat of the thermal evaporation film machine, and evacuate to 10 -3 Pa, set the current to control the evaporation rate as The time is 6min, and the surface of the bamboo charcoal fiber cloth is plated with a layer of Ag nano crystal seeds, the average particle size is 4nm; c. 0.5mg polyvinylpyrrolidone, 5ml ethylene...

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Abstract

The invention provides an efficient and lasting antibacterial material and a preparation method thereof. The preparation method comprises the following steps: cleaning bamboo charcoal fiber cloth, treating under dielectric barrier discharge equipment, and evaporating Ag nanocrystalline crystal seeds; sequentially dissolving a certain amount of polyvinylpyrrolidone, ethylene glycol and succinic acid in deionized water to form a solution A, then adding the bamboo charcoal fiber cloth plated with a layer of Ag nano crystal seeds into the solution A, then dropwise adding a silver nitrate solution with a certain concentration, intensely stirring, and meanwhile, gradually heating to a certain temperature to obtain the bamboo charcoal fiber cloth (at) Ag; and carrying out ball-milling crushing, removing an unattached Ag material and the like to obtain the efficient and lasting antibacterial material with uniform particles and high combination degree. The method is simple in preparation process, low in equipment requirement, high in controllable degree and capable of remarkably improving the combination degree of the Ag nano material and a carrier (bamboo charcoal fiber), so that the antibacterial effect is lasting and efficient, and the method is widely applied to the fields of the clothing industry, the chemical industry and the like.

Description

technical field [0001] The invention belongs to the technical field of nanometer material and preparation technology of clothing industry, and relates to a high-efficiency and durable antibacterial material and a preparation method thereof. Background technique [0002] With the rapid development of social economy, people's awareness of antibacterial health care in the living environment is gradually strengthened. In order to effectively and reasonably prevent antibiotics from being abused, excellent functional antibacterial materials have become daily necessities. At present, functional antibacterial materials can be classified into organic antibacterial materials and inorganic antibacterial materials according to their chemical composition. Organic antibacterial materials have the advantages of fast sterilization and high efficiency, but they have disadvantages such as poor heat resistance, easy hydrolysis, short validity period, and large side effects. At present, the saf...

Claims

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Application Information

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IPC IPC(8): B22F1/02B22F9/04C23C14/18C23C14/24C23C18/44A01N59/16A01N25/08A01P1/00A01P3/00
CPCB22F9/04C23C14/18C23C14/24C23C18/44A01N59/16A01N25/08B22F2009/043B22F1/17
Inventor 周华挺刘兰芳吴小平
Owner 瑞安铭恩科技有限公司
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