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A high-temperature high-emissivity infrared radiation coating and its preparation method and application method

An infrared radiation coating and high-emissivity technology, which is applied in the field of high-temperature high-emissivity infrared radiation coating and its preparation, can solve the problems of short effective working time of infrared radiation coating, easy growth of nano-powder, and rapid decay of emissivity, etc. Problems, to achieve the effect of low cost, long service life, convenient spraying

Active Publication Date: 2022-04-15
WUHAN UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, nanopowders are easy to grow or react with impurities in the use environment at high temperatures, and their emissivity decays quickly at high temperatures
[0006] "A high-performance infrared radiation coating for industrial kilns" (CN201710706569.3). Although the infrared radiation coating prepared by this technology has a high infrared radiation rate and a high refractory temperature, most industrial kilns are very It is difficult to isolate the air. The graphene in the infrared radiation coating is very easy to oxidize, and once oxidized, its emissivity drops rapidly; and BN in the infrared radiation agent is also very easy to oxidize in high-temperature air, and its oxidation products and SiO 2 , Mn 2 o 3 , Fe 2 o 3 Such components are very easy to react to form a low-melting liquid phase, resulting in a very short effective working time of the infrared radiation coating at high temperatures

Method used

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  • A high-temperature high-emissivity infrared radiation coating and its preparation method and application method
  • A high-temperature high-emissivity infrared radiation coating and its preparation method and application method
  • A high-temperature high-emissivity infrared radiation coating and its preparation method and application method

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Embodiment 1

[0037] A high-temperature and high-emissivity infrared radiation coating and its preparation method and application method. The preparation method described in this embodiment and the method of use are:

[0038]

[0039]

[0040] According to the raw materials and content of the high-temperature high-emissivity infrared radiation coating, mixing with a planetary ball mill, the ball-to-material ratio is 2-3:1, and mixing for 0.5-1 hour to obtain the high-temperature high-emissivity infrared radiation coating.

[0041] The preparation method of described CuO doped magnesium chromium spinel fine powder is:

[0042] Magnesium oxide, copper oxide and chromium oxide are used as raw materials, the raw materials are placed in a planetary ball mill, absolute ethanol is used as a ball milling medium, ball milled for 8-9 hours, dried, and pressed into a green body under the condition of 10-20 MPa. Insulate at 1150-1250°C for 3-4 hours, cool naturally with the furnace, crush, and s...

Embodiment 2

[0048] A high-temperature and high-emissivity infrared radiation coating and its preparation method and application method. The preparation method described in this embodiment and the method of use are:

[0049]

[0050] According to the raw materials and content of the high-temperature high-emissivity infrared radiation coating, mixing with a planetary ball mill, the ball-to-material ratio is 2-3:1, and mixing for 1-1.5 hours to obtain the high-temperature high-emissivity infrared radiation coating.

[0051] The preparation method of described CuO doped magnesium chromium spinel fine powder is:

[0052] Using magnesium oxide, copper oxide and chromium oxide as raw materials, putting the raw materials in a planetary ball mill, using absolute ethanol as a ball milling medium, ball milling for 9-10 hours, drying, and pressing under the condition of 20-30MPa to form a green body. Insulate at 1250-1350°C for 4-5 hours, cool naturally with the furnace, crush, and sieve to a par...

Embodiment 3

[0058] A high-temperature and high-emissivity infrared radiation coating and its preparation method and application method. The preparation method described in this embodiment and the method of use are:

[0059]

[0060] According to the raw materials and content of the high-temperature high-emissivity infrared radiation coating, mixing with a planetary ball mill, the ball-to-material ratio is 3-4:1, and mixing for 1-1.5 hours to obtain the high-temperature high-emissivity infrared radiation coating.

[0061] The preparation method of described CuO doped magnesium chromium spinel fine powder is:

[0062] Using magnesium oxide, copper oxide and chromium oxide as raw materials, placing the raw materials in a planetary ball mill, using absolute ethanol as a ball milling medium, ball milling for 10-11 hours, drying, and pressing under the condition of 25-35 MPa to form a green body. Insulate at 1300-1400°C for 4-5 hours, cool naturally with the furnace, crush, and sieve to a p...

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Abstract

The invention relates to a high-temperature and high-emissivity infrared radiation coating, a preparation method and a use method thereof. The technical scheme is as follows: the CuO-doped magnesia-chromium spinel fine powder, silicified expanded graphite, Guangxi white mud, elemental silicon powder, glass powder, silica sol, glycerol and citric ammonium nitrate are mixed with a planetary ball mill to obtain high temperature and high emission. rate infrared radiation coatings. The use method of the high-temperature and high-emissivity infrared radiation coating is as follows: by brushing or spraying, the high-temperature and high-emissivity infrared radiation coating is evenly coated on the surface of the industrial furnace wall, air-dried, and dried at 110-700 °C. Heat treatment under the condition of ℃ for 1 to 4 hours to obtain a high temperature and high infrared radiation coating. The invention has the advantages of low cost, simple process and convenient spraying, and has the characteristics of high infrared radiation rate in the 1-5 μm band and long service life in industrial furnaces above 1000° C. and without air isolation.

Description

technical field [0001] The invention belongs to the technical field of high-temperature and high-emissivity infrared radiation coatings. In particular, it relates to a high-temperature and high-emissivity infrared radiation coating and its preparation method and application method. Background technique [0002] The energy consumption of industrial furnaces used in high-temperature industries is huge. Among the high-temperature energy generated by the heat source of industrial furnaces, workpieces or products are heated mainly through two heat transfer methods: heat convection and heat radiation. In a high-temperature industrial environment greater than 800°C, the theoretical proportion of radiation heat transfer is more than 80% among the three heat transfer methods (radiation, convection, and conduction). Especially for high-temperature flame furnaces with large actual consumption and high energy consumption, the form of radiation heat transfer is the absolute dominant for...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D1/00C09D7/61C09D7/63
CPCC09D1/00C09D7/61C09D7/63
Inventor 桑绍柏武奇王光阳李亚伟王庆虎朱天彬
Owner WUHAN UNIV OF SCI & TECH
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