Method for improving heat stability of anthocyanin based on rice glutelin nanofibers
A nanofiber and gluten technology, applied in the functions of food ingredients, food ingredients containing natural extracts, food science, etc., can solve problems such as unclear structure and need for further research on physiological activity, and achieve improved retention rate, anthocyanins, etc. Effects of improved thermal stability and high specific surface area
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Embodiment 1
[0041] A preparation method of rice gluten nanofibers, comprising the steps of:
[0042] (1) Disperse the rice gluten in deionized water containing 150mM NaCl to obtain a rice gluten solution with a mass concentration of 4%, and then adjust the rice gluten solution to pH=2 with 1M HCl;
[0043] (2) Stir the rice gluten solution with pH=2 obtained in step (1) at a speed of 300r / min for 2h, and place it in a 4°C refrigerator for hydration for 12h to ensure sufficient hydration; Heating in a water bath for 24 hours at ℃; cooling in an ice bath for 20 minutes after heating to obtain rice glutenin nanofibers (atomic force microscope as shown in figure 1 ).
Embodiment 2
[0045] A method for improving the thermal stability of anthocyanins based on rice gluten nanofibers, comprising the steps of:
[0046] (1) Disperse cyanidin-3-O-glucoside into water to obtain a 5 mM anthocyanin solution, and then store it in the dark at 4°C for later use;
[0047] (2) The rice glutenin nanofibers obtained in Example 1 were dialyzed in pH 2 water for 24 hours using a 500D dialysis bag, and the water was changed every 4 hours. The protein concentration was adjusted slightly with pH 2 deionized water to obtain a pH of 2. Concentration is the rice glutenin nanofiber solution (the fiber solution that obtains through dialysis) of 20mg / mL;
[0048] (3) Mix the anthocyanin solution obtained in step (1) and the rice glutenin nanofiber solution obtained in step (2) according to a volume ratio of 1:1, adjust the pH to 3, and stir at a speed of 300r / min for 30min to obtain anthocyanin -Rice glutenin nanofiber composite (atomic force microscopy image shown in figure 2 )...
Embodiment 3
[0049] The optimization of embodiment 3pH
[0050] Adjust the pH in step (3) of Example 2 to be 5, 7, and keep the others consistent with Example 2 to obtain anthocyanin-rice glutenin nanofiber composites.
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