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Black pigment for ceramic ink-jet printing and preparation method and application thereof

A black pigment and ceramic inkjet technology, applied in the field of ceramic pigments, can solve problems such as unstable color development, achieve the effects of improving glaze defects, increasing crystallinity, improving color development performance and glaze defects

Active Publication Date: 2021-11-02
FOSHAN SANSHUI CREATE TIDE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] One of the purposes of the present invention is to overcome the deficiencies in the prior art, to provide a black pigment for inkjet printing of ceramics, to solve the problem of unstable color development and glaze defects (such as Chromatic aberration, yin and yang color, pinhole, white point) problems

Method used

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  • Black pigment for ceramic ink-jet printing and preparation method and application thereof
  • Black pigment for ceramic ink-jet printing and preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0044] A kind of preparation method of black pigment for ceramic inkjet printing of the present embodiment, comprises the following steps:

[0045] Step 1, the preparation of calcined material: the Cr 2 o 3 and Fe 2 o 3 Press m(Cr 2 o 3 ):m(Fe 2 o 3 )=2.0 for batching, put it in a mixer and stir evenly, then put it in a pusher kiln for firing, the firing temperature is 1220°C, the holding time is 9h, and then the prepared powder is crushed with a powder machine , until the fineness is 325 mesh full pass or smaller fineness, to obtain calcined material.

[0046] Step 2, the preparation of colorant: carry out batching with calcined material and remaining raw material according to formula, the weight parts of each raw material are as follows: calcined material is 27 parts, Co 3 o 4 27.5 parts for NiO, 30 parts for NiO, MnO 2 5 parts, Al 2 o 3 4 parts, SrCO 3 for 3 copies, Bi 2 o 3 For 2 parts, MoO 3 It is 1.5 parts. Put the ingredients in the mixer and stir them eve...

Embodiment 2

[0048] A kind of preparation method of black pigment for ceramic inkjet printing of the present embodiment, comprises the following steps:

[0049] Step 1, the preparation of calcined material: the Cr 2 o 3 and Fe 2 o 3 Press m(Cr 2 o 3 ):m(Fe 2 o 3 )=1.9 for batching, put it in a mixer and stir evenly, then put it in a pusher kiln for firing, the firing temperature is 1260°C, the holding time is 6.5h, and then the prepared powder is crushed with a powder machine Processing, until the fineness is 325 mesh all-through, to obtain calcined material.

[0050] Step 2, the preparation of colorant: carry out batching with calcined material and remaining raw material according to formula, the weight parts of each raw material are as follows: calcined material is 33.8 parts, Co 3 o 4 27.5 parts, NiO 30 parts, Al 2 o 3 4 parts, SrCO 3 1.2 parts, Bi 2 o 3 For 2 parts, MoO 3 It is 1.5 parts. Put the ingredients in a mixer and stir evenly, then put them in a pusher kiln for ...

Embodiment 3

[0052] A kind of preparation method of black pigment for ceramic inkjet printing of the present embodiment, comprises the following steps:

[0053] Step 1, the preparation of calcined material: the Cr 2 o 3 and Fe 2 o 3 Press m(Cr 2 o 3 ):m(Fe 2 o 3 )=2.1 for batching, put it in a mixer and stir evenly, then put it in a pusher kiln for firing, the firing temperature is 1230°C, the holding time is 6h, and then the prepared powder is crushed with a powder machine , until the fineness is 325 mesh full pass or smaller fineness, to obtain calcined material.

[0054] Step 2, the preparation of colorant: carry out batching with calcined material and remaining raw material according to formula, the weight parts of each raw material are as follows: calcined material is 17 parts, Co 3 o 4 32.3 parts for NiO, 45 parts for NiO, MnO 2 2 parts, SrCO 3 2.2 parts, Bi 2 o 3 For 1 part, MoO 3 0.5 parts, put the ingredients in a mixer and stir evenly, then put them in a pusher kiln...

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Abstract

The invention belongs to the technical field of ceramic pigments, and particularly relates to a black pigment for ceramic ink-jet printing and a preparation method and application thereof. The black pigment is prepared from the following raw materials in parts by weight: 17-35 parts of a pre-sintered material, 25-36 parts of Co3O4, 30-45 parts of NiO, 0-5 parts of MnO2, 0-4 parts of Al2O3, 0-3 parts of SrCO3, 0-2 parts of Bi2O3 and 0.5-1.5 parts of MoO3, wherein the pre-sintered material is a material formed by sintering a mixed material of Cr2O3 and Fe2O3. Through cooperation of the raw materials, the problems of unstable color development and glaze defects (such as chromatic aberration, color shading, pinholes and white dots) after ink is prepared from the existing black pigment can be solved, the color development performance of black ceramic ink can be improved, and glaze defects can be reduced.

Description

technical field [0001] The invention relates to the technical field of ceramic coloring materials, in particular to a black coloring material for inkjet printing of ceramics and its preparation method and application. Background technique [0002] After less than ten years of development, ceramic inkjet printing technology has basically replaced traditional printing technology. In recent years, tile products with gray, white and black patterns have become popular. This design style has been widely used in fully glazed, antique tiles and ceramic rock slab products, which has led to an increase in the use of black ink. [0003] Existing black pigments, such as a Cu-Mn-Fe-Cr cobalt-free black ceramic pigment and its preparation method disclosed in application number CN201310213944.2, and a kind of tannery sludge disclosed in application number CN202010541428.2 The method for preparing black cobalt-based ceramic pigments is to use raw materials cobalt oxide, chromium oxide, nic...

Claims

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Application Information

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IPC IPC(8): C09D11/32
CPCC09D11/32
Inventor 廖仲恩田秀娟张天杰周军张丹王祥乾戴建斌喻友军刘腾肖永平
Owner FOSHAN SANSHUI CREATE TIDE
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