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A kind of cerium oxide reflective thermal insulation coating and preparation method thereof

A technology of reflective heat-insulating coatings and cerium oxide, which is applied in the direction of reflection/signal coatings, anti-fouling/underwater coatings, coatings, etc., can solve the problems of heat insulation effect decline, coating reflectivity reduction, temperature rise, etc., to achieve durability Effects of improved stain resistance, improved reflectivity, and low reflectivity

Active Publication Date: 2022-08-02
TIANJIN BAOGANG RES INST OF RARE EARTHS +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

After adding color paste or inorganic pigments, the reflectivity of the paint will decrease, and the heat insulation effect will decrease significantly, causing the temperature of the surface and interior of the building to rise under the irradiation of sunlight

Method used

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  • A kind of cerium oxide reflective thermal insulation coating and preparation method thereof
  • A kind of cerium oxide reflective thermal insulation coating and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] The preparation method of primer comprises the following steps:

[0033] 200 g of deionized water, 8 g of a predispersant, and 400 g of cerium oxide were pre-dispersed with stirring, and ground with a sand mill for 15 minutes until the cerium oxide D(90) in the slurry was 1.2 μm. The above slurry is mixed with 300g of water-based pure acrylic emulsion, 8g of dispersant, 5g of wetting agent, 5.5g of defoamer, 1.5g of multifunctional auxiliary, 30g of film-forming auxiliary, and 3g of anti-settling agent in a dispersing machine. The line speed was controlled at 8 m / s, stirred for 35 minutes, added with 2.5 g of a pH adjuster, and stirred for 5 minutes to obtain a cerium oxide reflective heat-insulating paint primer.

[0034] The preparation method of topcoat comprises the following steps:

[0035] 200 g of deionized water, 6 g of pre-dispersant, 100 g of iron oxide yellow pigment, and 300 g of cerium oxide were stirred and pre-dispersed, and ground with a sand mill for 1...

Embodiment 2

[0039] The preparation method of the primer is the same as that in Example 1.

[0040] The preparation method of topcoat comprises the following steps:

[0041] 300 g of deionized water, 6 g of pre-dispersant, 80 g of red iron oxide pigment, and 320 g of cerium oxide were stirred and pre-dispersed, and ground with a sand mill for 10 minutes until the pigment particle size D(90) in the slurry was 1.5 μm. The red slurry is mixed with 300g of water-based pure acrylic emulsion, 8g of dispersant, 5g of wetting agent, 5.5g of defoamer, 1.5g of multifunctional auxiliary agent, 30g of film-forming auxiliary agent, and 3g of anti-settling agent in a dispersing machine. The line speed was controlled at 8 m / s, stirred for 35 minutes, added with 2.5 g of a pH adjuster, and stirred for 5 minutes to obtain a brick red reflective heat-insulating paint finish B.

[0042] The test sample is first sprayed with a layer of primer with a thickness of 0.1mm ~ 0.15mm, and then sprayed with a layer ...

Embodiment 3

[0045] The preparation method of the primer is the same as that in Example 1.

[0046]The preparation method of topcoat comprises the following steps:

[0047] 300 g of deionized water, 6 g of pre-dispersant, 60 g of iron oxide green pigment, and 240 g of cerium oxide were stirred and pre-dispersed, and ground with a sand mill for 10 minutes until the pigment particle size D(90) in the slurry was 1.3 μm. The above green slurry is mixed with 300g of water-based pure acrylic emulsion, 8g of dispersant, 5g of wetting agent, 5.5g of defoamer, 1.5g of multifunctional auxiliary, 30g of film-forming auxiliary, and 3g of anti-settling agent in a dispersing machine. , the line speed was controlled at 8m / s, stirred for 35 minutes, added 2.5g of pH adjuster, and stirred for 5 minutes to obtain green reflective thermal insulation paint topcoat 3.

[0048] The test sample is first sprayed with a layer of primer with a thickness of 0.1mm ~ 0.15mm, and then sprayed with a layer of topcoat C...

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Abstract

The invention provides a cerium oxide reflective heat-insulating paint and a preparation method thereof, comprising a primer layer and a topcoat layer, wherein the primer layer includes the following components: primer cerium oxide, a first water-based resin, a first pre-dispersed paint agent, first auxiliary agent, deionized water; the topcoat layer includes the following components in mass percentage: the second water-based resin, the second pre-dispersant, the second auxiliary agent, the topcoat cerium oxide, the infrared reflective pigment, the deionized Ionized water. The cerium oxide and pigments used in the coating of the present invention have high reflectance of visible light and near-infrared light, and the coating layer has high reflectance of sunlight, near-infrared reflectance and hemispherical emissivity, which can effectively reflect and block solar radiation, Reduce building surface and interior temperatures.

Description

technical field [0001] The invention belongs to the field of coatings and preparations thereof, in particular to a cerium oxide reflective heat-insulating coating and a preparation method thereof. Background technique [0002] Among rare earth elements, cerium is the most abundant in nature. Cerium oxide is a material with great application potential, which is widely used in catalysis, anticorrosion, photocatalysis, ultraviolet absorber, thermal insulation coating and glass abrasives, etc., which is attributed to the special physical and chemical properties of cerium. Patent CN103333581B discloses the application of nano-cerium oxide in coating epoxy composite coatings. After nano-cerium oxide is modified by titanate coupling agent, the addition amount in the coating does not exceed 10%, so that the coating has good anti-corrosion properties. performance. Patent CN109852177A discloses adding cerium oxide to thermal insulation ceramic coating to solve the problem of crackin...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D133/04C09D5/33C09D5/00C09D5/14
CPCC09D133/04C09D5/004C09D5/002C09D5/14C08K2003/2213C08K2003/2272C08K3/22
Inventor 张呈祥张秀荣刘威郝先库张光睿赵长玉李璐彭维温永清王安丽周鑫喆
Owner TIANJIN BAOGANG RES INST OF RARE EARTHS