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Coal gasification grey water dispersing agent and preparation method thereof

A dispersant and gray water technology, applied in chemical instruments and methods, descaling and water softening, water/sludge/sewage treatment, etc., can solve facility scaling and blockage, impact on production capacity and benefits, and affect the safety and stability of production equipment Operation and other problems, to achieve continuous and stable operation, excellent results

Pending Publication Date: 2021-12-21
南京开广化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The commonly used scale inhibitors and dispersants in the gray and black water treatment of the former coal gasification unit are generally not ideal, resulting in scaling and blockage of the quenching ring of the gasification chamber, gray water heat exchanger tubes, gray water pumps and other facilities. In severe cases, production must be shut down The cleaning will greatly affect the safe and stable operation of the production equipment, and the production capacity and benefits will be greatly affected
[0003] Patent CN201811131451.3 discloses a non-phosphorus scale inhibitor dispersant for coal gasification gray water, which can prevent scaling of equipment pipes in coal gasification gray water system, control inorganic salt scale, metal oxides and colloidal precipitation, but its stability is not good. High, poor high temperature resistance

Method used

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  • Coal gasification grey water dispersing agent and preparation method thereof
  • Coal gasification grey water dispersing agent and preparation method thereof
  • Coal gasification grey water dispersing agent and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment

[0029] (1) Picking materials: 150kg of tricarboxylic butane phosphate, 100kg of polymaleic anhydride, 150kg of acrylic acid-acrylamide sulfonate binary copolymer, and 600kg of tap water.

[0030] (2) Feeding: Inhale tap water into a 3T reactor, keep the temperature at 30-40°C, and start stirring; put tricarboxylic butane phosphate and polymaleic anhydride into the reactor in turn, and add acrylic acid-acrylamide sulfonate The binary copolymer is sucked into the reactor, stirred for 30 minutes, and mixed evenly;

[0031] (3) Stand still: After standing still for 30 minutes, cool to normal temperature, take a sample and check that there is no precipitation after precipitation;

[0032] (4) Filtration: the finished product is obtained after filtration and packaging.

[0033] Such as figure 1 It can be seen from the dispersion rate test chart that the dispersion rate test conditions are 200mg / L calcium hydride, 200mg / L bicarbonate, 2000 200mg / L black water suspension, pH 8.8, au...

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PUM

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Abstract

The invention discloses a coal gasification grey water dispersing agent and a preparation method thereof, the coal gasification grey water dispersing agent comprises 5%-15% of phosphoric acid tricarboxylic acid butane, 5%-15% of polymaleic anhydride, 5%-15% of acrylic acid-acrylamide sulfonate biopolymer and tap water, and the preparation method comprises the steps of material picking, feeding, standing and filtering. According to the present invention, the high-temperature scale inhibition dispersion effect is excellent, the scale inhibition dispersion rate of more than 80% at the high temperature of more than 200 DEG C is still maintained, the scale inhibition dispersion agent has been applied to a variety of gasification furnaces such as coal water slurry gasification, pulverized coal gasification and the like, can be used for a long enough period, can not be stopped for more than 6 months, and can ensure the continuous and stable operation of the device.

Description

technical field [0001] The invention belongs to the field of chemical industry, and in particular relates to a coal gasification ash water dispersant and a preparation method thereof. Background technique [0002] The commonly used scale inhibitors and dispersants in the gray and black water treatment of the former coal gasification unit are generally not ideal, resulting in scaling and blockage of the quenching ring of the gasification chamber, gray water heat exchanger tubes, gray water pumps and other facilities. In severe cases, production must be shut down The cleaning will greatly affect the safe and stable operation of the production equipment, and the production capacity and benefits will be greatly affected. [0003] Patent CN201811131451.3 discloses a non-phosphorus scale inhibitor dispersant for coal gasification gray water, which can prevent scaling of equipment pipes in coal gasification gray water system, control inorganic salt scale, metal oxides and colloidal...

Claims

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Application Information

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IPC IPC(8): C02F5/14
CPCC02F5/14C02F2303/08
Inventor 金玉泉
Owner 南京开广化工有限公司
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