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Method for removing gentiana straminea polysaccharide pigment by using three-dimensional porous amino graphene decolorizing column

An aminographene, three-dimensional porous technology is applied in the field of three-dimensional porous aminographene decolorization column to remove the polysaccharide pigment of P. chinensis, which can solve problems such as low efficiency and low decolorization rate, and achieve high decolorization rate and recovery rate and high decolorization efficiency , the effect of high polysaccharide retention rate

Active Publication Date: 2022-01-11
NORTHWEST A & F UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The object of the present invention is to overcome the shortcoming of above-mentioned prior art, provide a kind of method that three-dimensional porous amino-graphene decolorization column removes genus polysaccharide pigment, this method carries out decolorization treatment to genus polysaccharide by using three-dimensional porous amino-graphene decolorization column , to solve the problem of low decolorization rate and low efficiency in the static test process of polysaccharide decolorization in the prior art

Method used

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  • Method for removing gentiana straminea polysaccharide pigment by using three-dimensional porous amino graphene decolorizing column
  • Method for removing gentiana straminea polysaccharide pigment by using three-dimensional porous amino graphene decolorizing column
  • Method for removing gentiana straminea polysaccharide pigment by using three-dimensional porous amino graphene decolorizing column

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Experimental program
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Effect test

Embodiment 1

[0036] Step 1, using natural graphite as a material, after preparing graphene oxide by the classic Hummers method, prepare a graphene oxide solution with a concentration of 6 mg / mL; mix the graphene oxide solution and ethylene dioxide with a concentration of 6 mg / mL in volume ratio Amine, the mixed solution A is prepared, the mixing ratio is graphene oxide solution: ethylenediamine=200:1.2, the mixed solution A is ultrasonicated for 10min, and then transferred to an autoclave with a polytetrafluoroethylene liner, at 120 ° C After reacting for 14 hours, a three-dimensional porous amino-graphene hydrogel was obtained, which was washed with deionized water and loaded into a chromatogram to obtain a three-dimensional porous amino-graphene decolorization column.

[0037] Step 2. Dissolve the washed Gentiana in distilled water according to the solid-liquid ratio of 1g: (10-20)mL to obtain mixture B. Ultrasonic extract the mixture B for 3 times, collect and combine the extractions of ...

Embodiment 2

[0043] Step 1, using natural graphite as a material, after preparing graphene oxide by the classic Hummers method, prepare a graphene oxide solution with a concentration of 6 mg / mL; mix the graphene oxide solution and ethylene dioxide with a concentration of 6 mg / mL in volume ratio Amine, to prepare a mixed solution A, the mixing ratio is graphene oxide solution: ethylenediamine = 200: 1.2, the mixed solution A ultrasonic 10min, and then transferred to a polytetrafluoroethylene lined autoclave, at 120 ° C After reacting for 14 hours, a three-dimensional porous amino-graphene hydrogel was obtained, which was washed with deionized water and loaded into a chromatogram to obtain a three-dimensional porous amino-graphene decolorization column.

[0044] Step 2. Dissolve the washed Gentiana in distilled water according to the solid-liquid ratio of 1g: (10-20)mL to obtain mixture B. Ultrasonic extract the mixture B for 3 times, collect and combine the extractions of the 3 extractions ...

Embodiment 3

[0050] Step 1, using natural graphite as a material, after preparing graphene oxide by the classic Hummers method, prepare a graphene oxide solution with a concentration of 6 mg / mL; mix the graphene oxide solution and ethylene dioxide with a concentration of 6 mg / mL in volume ratio Amine, to prepare a mixed solution A, the mixing ratio is graphene oxide solution: ethylenediamine = 200: 1.2, the mixed solution A ultrasonic 10min, and then transferred to a polytetrafluoroethylene lined autoclave, at 120 ° C After reacting for 14 hours, a three-dimensional porous amino-graphene hydrogel was obtained, which was washed with deionized water and loaded into a chromatogram to obtain a three-dimensional porous amino-graphene decolorization column.

[0051] Step 2. Dissolve the washed Gentiana in distilled water according to the solid-liquid ratio of 1g: (10-20)mL to obtain mixture B. Ultrasonic extract the mixture B for 3 times, collect and combine the extractions of the 3 extractions ...

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Abstract

The invention discloses a method for removing gentiana straminea polysaccharide pigment by using a three-dimensional porous amino graphene decolorizing column. According to the method, three-dimensional porous amino graphene hydrogel is loaded into a chromatographic column to prepare the decolorizing column, then the decolorizing column is applied to the field of gentiana straminea polysaccharide pigment removal, the application and removal process is simple, and the method is economical, and the cost is appropriate; the prepared three-dimensional porous amino graphene decolorizing column is successfully applied to decolorization of various polysaccharides, the decolorization rate and the recovery rate are very high, the decolorization efficiency in the removal process is high, and the polysaccharide retention rate is high. Besides, the three-dimensional porous amino graphene decolorizing column provides superior practical functions, exceeds many traditional methods, and overcomes the problems of use of organic reagents, difficulty in reuse and the like. Tests prove that when the gentiana straminea polysaccharide is decolored by the method, the decoloring efficiency is more than 95%, and the polysaccharide retention rate is more than 95%.

Description

technical field [0001] The invention belongs to the field of refining and processing methods of plant active ingredients, and in particular relates to a method for removing genita polysaccharide pigments by a three-dimensional porous amino graphene decolorization column. Background technique [0002] Gentiana is a traditional Chinese medicinal material, belonging to the four authentic raw materials of Gentiana chinensis. Gentiana grows in Tibet, Qinghai, Sichuan and other places, and is popular on the Qinghai-Tibet Plateau. It is called "Xiejigabao" in Tibetan. At present, there have been many literature reports that the root of Gentiana twista is commonly used to treat rheumatism, damp-heat jaundice and so on. In Korea, Gentiana has been recorded as an active substance used in the production of functional food and pharmaceutical industries to improve age-related osteoarthritis. Due to the rapidly aging population, the demand for Gentiana is growing. The previous research...

Claims

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Application Information

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IPC IPC(8): C08B37/00
CPCC08B37/0003
Inventor 王建龙石硕张文涛蓝熙冯建兴
Owner NORTHWEST A & F UNIV
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