An environment-friendly food packaging film production technology with accelerated freezing function
A technology of food packaging film and production technology, which is applied in the field of food packaging materials, can solve the problem of single function of film materials, and achieve the effect of reducing supercooling temperature
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Embodiment 1
[0021]According to the well-known method, wheat bran is deenzed, crushed, de-starched and deproteinized, and then compared with 1.5M NaOH and 2.0M urea mixture is evenly mixed, formulated into a mass volume concentration of 5% of the mixture, stirred at 25 ° C for 8 ~ 12 h, after the end of the reaction at 5000 rpm centrifugation for 10 min to take the supernatant; anhydrous ethanol is added to the solution to a volume concentration of 40%, 8000 rpm centrifugation 20 min to take the supernatant, continue to add anhydrous ethanol to the volume concentration to 50%, repeat the centrifugation process, to obtain a polysaccharide precipitate at a 50% ethanol volume concentration; the precipitation is resuspended with pure water, dialyzed at 4 °C for 48 to 72 h, and the resulting solution is lyophilized to prepare a 50% alcohol concentration of AX ; Dissolve AX in dimethyl sulfoxide and formulate into a solution with a mass volume concentration of 4%; Adjust the pH of the solution to 8....
Embodiment 2
[0023]Wheat bran AX extraction process is the same as Example 1, the alcohol deposit concentration is 30%; Triethylamine solution pH adjusted to 8.0, AX and OSA molar ratio of 2, centrifugation, precipitation, rinsing, dry coal process with Example 1; The modified AX is formulated into a solution with a mass volume concentration of 2%, degassing, casting film, drying process with Example 1; AX soaking with Example 1, adding a volume concentration of 0.06% trichlorovinyl silane solution, reaction, rinsing, drying process with Example 1; AX base film and butanthiol light control reaction process is the same as Example 1, ultraviolet treatment conditions of 300W power irradiation for 4min, rinsing, drying process with Example 1; Α-Al with a particle size of 10 nm 2 O 3 The particles are mixed with 50mL hexane, formulated into a solution with a mass volume concentration of 0.2%, silicone rubber mixing, ultrasonic, spraying, drying process with Example 1; The surface of the membrane ca...
Embodiment 3
[0025] Wheat bran AX extraction process is the same as Example 1, the alcohol sediment concentration is 70%; Triethylamine solution pH adjusted to 9.0, AX and OSA molar ratio of 12, centrifugation, precipitation, rinsing, drying process with Example 1; The modified AX is formulated into a solution with a mass volume concentration of 4%, degassing, casting film, drying process with Example 1; AX soaking with Example 1, adding a volume concentration of 0.12% trichlorovinylsilane solution, reaction, rinsing, drying process with Example 1; AX base film and butanethiol light control reaction process is the same as Example 1, ultraviolet treatment conditions of 500W power irradiation for 7min, rinsing, drying process with Example 1; A α-Al with a particle size of 30 nm 2 O 3 The particles are mixed with 50mL hexane, formulated into a solution with a mass volume concentration of 0.4%, silicone rubber mixing, ultrasonic, spraying, drying process with Example 1; The surface of the membrane...
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