Composite demineralized bone matrix composition containing bone mineral component and method for producing same
A technology of composite demineralized bone and bone inorganic matter, applied in bone implants, tissue regeneration, medical science and other directions, can solve the problems of undisclosed methods, loss, etc., to achieve biocompatibility, excellent bone formation effect, Excellent effect of osteoconductivity and osteoinductivity
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[0038] The present invention relates to the preparation method of compound demineralized bone matrix (DBM) complex composition by one-step method, it is characterized in that, comprises the following steps:
[0039] Decalcification step, using an acid solution to decalcify the bone tissue;
[0040] The bone inorganic matter precipitation step is to neutralize the decalcification-treated decalcification solution with an alkaline solution to precipitate bone inorganic matter;
[0041] BMP-2 extraction step, centrifuging the above precipitated solution, adding an acid solution to the precipitate to extract BMP-2; and
[0042] In the preparation step of the composite decalcified bone composition, the solution extracted from the above-mentioned BMP-2 is neutralized with an alkaline solution, and the decalcified bone, bone inorganic matter and BMP-2 are separated out.
[0043] Through the examples of the present invention, the composite decalcified bone composition is prepared by a...
Embodiment approach
[0140] Hereinafter, the present invention will be described more specifically by way of examples. However, the scope of the present invention is not limited to the following examples, and those skilled in the art can understand that various variations, modifications, or applications can be made without departing from the technical idea derived from the idea described in the claims.
Embodiment 1
[0142] Example 1. Obtaining composite demineralized bone composition by one-step method
[0143] With isopropanol (2-Propanol for analysis ACS, ISO, Reag. Ph Eur, Merck) washed the cortical bone, and then performed a pretreatment process of washing with sterilized distilled water.
[0144] Thereafter, 1 g of cortical bone was decalcified at room temperature for 4 hours using 10 to 50 ml of 0.5 to 1.5 normality (N) hydrochloric acid solution (Hydrochloric acid 35.0-37.0%, JUNSEI CHEMICAL CO., LTD.). After the above-mentioned decalcification is completed, use 0.5 to 4.0 M sodium hydroxide (NaOH, Sodiumhydroxide, Merck) solution in the mixed solution composed of supernatant and sediment to induce the precipitation of bone inorganic matter in the mixed solution, so that it can be combined with decalcified bone Precipitate together. Centrifuge the mixed solution that has completed precipitation and precipitation at 1000 to 8000 rpm for 10 to 30 minutes, and remove the supernatan...
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