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Production process and equipment of large-particle ammonium sulfate product

A production equipment and ammonium sulfate technology, applied in the field of large-grain ammonium sulfate production, can solve the problems of inability to produce large-grain ammonium sulfate feces, incapable of production, inconvenient adjustment and control, etc., to achieve full utilization of reaction heat and convenient operation , The addition of material is accurate and convenient

Active Publication Date: 2022-03-15
连云港钧格环境科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] However, during the use of the existing production equipment for large-grain ammonium sulfate products, it is not possible to quickly and high-quality produce and process large-grain ammonium sulfate feces, and it is inconvenient to adjust and control in the process of making large-grain ammonium sulfate. Due to the rapid production and manufacturing of streamlined, a production process and equipment for large-grained ammonium sulfate products are needed to solve the above-mentioned problems

Method used

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  • Production process and equipment of large-particle ammonium sulfate product
  • Production process and equipment of large-particle ammonium sulfate product
  • Production process and equipment of large-particle ammonium sulfate product

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0049] A large particle ammonium sulfate product such as figure 1 As shown, its production process includes the following steps:

[0050] S1. First add sulfuric acid, ammonia and the washing liquid from the gas-liquid separator into the tubular reactor for neutralization reaction. The slurry formed after the reaction is sprayed into the granulator, and sprayed into the solid material bed through the nozzle Granulation binder, and then spray ammonia for granulation to form solid wet material and granulation tail gas, wherein the granulation temperature is 80°C, and the water content of the solid wet material at the outlet of the granulator is 3%;

[0051] S2. The tail gas after granulation enters the gas-liquid separator and the washing liquid from the circulating pump of the gas-liquid separator is fully atomized and mixed in the Venturi injector. The gas-liquid mixture enters the gas-liquid separator for separation, and the washing liquid passes through the circulating pump a...

Embodiment 2

[0057] A large particle ammonium sulfate product such as figure 1 As shown, its production process includes the following steps:

[0058] S1. First add sulfuric acid, ammonia and the washing liquid from the gas-liquid separator into the tubular reactor for neutralization reaction. The slurry formed after the reaction is sprayed into the granulator, and sprayed into the solid material bed through the nozzle Granulation binder, and then spray ammonia for granulation to form solid wet material and granulation tail gas, wherein the granulation temperature is 90°C, and the water content of the solid wet material at the outlet of the granulator is 4%;

[0059] S2. The tail gas after granulation enters the gas-liquid separator and the washing liquid from the circulating pump of the gas-liquid separator is fully atomized and mixed in the Venturi injector. The gas-liquid mixture enters the gas-liquid separator for separation, and the washing liquid passes through the circulating pump a...

Embodiment 3

[0065] A large particle ammonium sulfate product such as figure 1 As shown, its production process includes the following steps:

[0066] S1. First add sulfuric acid, ammonia and the washing liquid from the gas-liquid separator into the tubular reactor for neutralization reaction. The slurry formed after the reaction is sprayed into the granulator, and sprayed into the solid material bed through the nozzle Granulation binder, and then spray ammonia for granulation to form solid wet material and granulation tail gas, wherein the granulation temperature is 110°C, and the water content of solid wet material at the outlet of the granulator is 5%;

[0067] S2. The tail gas after granulation enters the gas-liquid separator and the washing liquid from the circulating pump of the gas-liquid separator is fully atomized and mixed in the Venturi injector. The gas-liquid mixture enters the gas-liquid separator for separation, and the washing liquid passes through the circulating pump and ...

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Abstract

The invention relates to the technical field of production of large-particle ammonium sulfate, in particular to a production process and equipment of a large-particle ammonium sulfate product, and the process comprises the following steps: firstly, carrying out neutralization reaction on sulfuric acid, ammonia and a washing solution from a gas-liquid separator, spraying slurry formed after the reaction into a granulator, spraying a granulation binder into the solid material bed through a spray head, and then spraying ammonia for granulation to form a solid wet material and granulation tail gas; the solid wet materials are dried, and the dried materials enter a screening machine to be graded; screening out qualified particles and directly cooling to obtain a large-particle ammonium sulfate product; the equipment comprises a gas-liquid separation device, a fixed supporting frame, a screening device and a feeding reaction device. According to the invention, the large granulation of ammonium sulfate is realized, the tubular reactor is sufficient in reaction heat utilization and short in reaction time, the production cost of the large-particle ammonium sulfate can be properly reduced, certain direct economic benefits are achieved, the process conditions are easy to control, the operation is convenient, and the product quality is good.

Description

technical field [0001] The invention relates to the technical field of large-grain ammonium sulfate production, in particular to a production process and equipment for large-grain ammonium sulfate products. Background technique [0002] Pure ammonium sulfate is a colorless transparent orthorhombic crystal, and its aqueous solution is acidic. Insoluble in alcohol, acetone and ammonia. It is hygroscopic, and will condense into blocks after absorbing moisture. When heated above 513°C, it can be completely decomposed into ammonia, nitrogen, sulfur dioxide and water. When reacting with alkalis, ammonia gas is released. React with barium chloride solution to form barium sulfate precipitate. Salting out of proteins can also occur. [0003] According to Chinese Patent No. CN201611115585.7, a method for producing large-grained ammonium sulfate, a method for producing large-grained ammonium sulfate, the method comprises the following steps: Step 1: producing the slurry produced i...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C05C3/00C05G3/20C05G5/12C01C1/242
CPCC05C3/00C05G3/20C05G5/12C01C1/242Y02P20/10
Inventor 王凯
Owner 连云港钧格环境科技有限公司