Thermosetting insulating oil as well as preparation method and application thereof
A technology of thermosetting insulation and curing agent, applied in the field of ink, can solve the problem of poor insulation of thermosetting ink
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Embodiment 1
[0046] 1) Weigh 8 parts by mass of Aekyung's TOTM plasticizer and 2 parts by mass of Eastman's TXIB plasticizer and pour them into a stirring tank, pass cooling water at 15°C, start stirring and control the temperature at 25°C, and continue in order Add the following materials:
[0047] a. Add 1 part by mass of Galata's MARK CZ11 calcium zinc stabilizer, stir for 1 min, and mix well;
[0048] b. Add 40 parts by mass of Hanwha's KCM-12PVC paste resin, stir for 8 minutes, and mix well;
[0049] c. Add 9 parts by mass of OK500 silica powder, stir for 4 minutes, and mix well;
[0050] d. Add 40 parts by mass of Guangxi Warner New Material Technology Co., Ltd. nano-calcium carbonate LLD-30 nano-calcium carbonate powder, stir for 12 minutes, and mix well;
[0051] 2) The homogeneous material prepared in step 1) is dispersed by using a three-roll machine for high-speed shearing and grinding to obtain a thermosetting insulating oil.
[0052] The viscosity of the above thermosetting...
Embodiment 2
[0057] 1) Weigh 15 parts by mass of Aekyung's TOTM plasticizer and 5 parts by mass of Eastman's TXIB plasticizer and pour them into a stirring tank, pass cooling water at 15°C, start stirring and control the temperature at 25°C, and continue in order Add the following materials:
[0058] a. Add 5 parts by mass of Galata's MARK CZ11 calcium zinc stabilizer, stir for 1 min, and mix well;
[0059] b. Add 25 parts by mass of Hanwha's KCM-12PVC paste resin, stir for 8 minutes, and mix well;
[0060] c. Add 10 parts by mass of OK500 silica powder, stir for 4 minutes, and mix well;
[0061] d. Add 40 parts by mass of Guangxi Warner New Material Technology Co., Ltd. nano-calcium carbonate LLD-30 nano-calcium carbonate powder, stir for 12 minutes, and mix well;
[0062] 2) The homogeneous material prepared in step 1) is dispersed by using a three-roll machine for high-speed shearing and grinding to obtain a thermosetting insulating oil.
[0063] Using a rheometer Malvern Kinexus to ...
Embodiment 3
[0068] 1) Weigh 20 parts by mass of Shandong Lanfan's DOTP plasticizer and 5 parts by mass of Eastman's TXIB plasticizer and pour them into the stirring tank, pass cooling water at 15°C, start stirring and control the temperature at 25°C, continue to press Add the following materials in order:
[0069] a. Add 5 parts by mass of Galata's MARK CZ11 calcium zinc stabilizer, stir for 1 min, and mix well;
[0070] b. Add 40 parts by mass of Hanwha's KCM-12PVC paste resin, stir for 8 minutes, and mix well;
[0071] c. Add 10 parts by mass of OK500 silica powder, stir for 4 minutes, and mix well;
[0072] d. Add 20 parts by mass of Guangxi Warner New Material Technology Co., Ltd. nano-calcium carbonate LLD-30 nano-calcium carbonate powder, stir for 12 minutes, and mix well;
[0073] 2) The homogeneous material prepared in step 1) is dispersed by using a three-roll machine for high-speed shearing and grinding to obtain a thermosetting insulating oil.
[0074] The viscosity of the abo...
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