Anti-stripping agent as well as preparation method and application thereof
An anti-stripping agent and anti-stripping technology, applied in the field of petroleum industry and basic material chemistry, to achieve the effects of reducing the incidence of flight accidents, improving adhesion strength, and good high-temperature peeling resistance
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Embodiment 1
[0043] The SBR with a combined styrene content of 23wt% was pulverized in advance, with a particle size of 5-19mm, and set aside. Warm up the kneader and set aside.
[0044] Weigh 2.0kg of pulverized SBR, 2.0kg of triphenylmethane triisocyanate, 2.0kg of N,N'-diphenyl-p-phenylenediamine, 1.0kg of silane coupling agent (KH560), and 3.0kg of four-line extraction oil Put it in a kneader for kneading, the kneading temperature is 130°C, and the kneading time is 60min; then extrude, the extrusion temperature is 110°C to obtain a pasty anti-stripping agent. The distribution ratio of each group is shown in Table 1.
Embodiment 2
[0046] The SBR with a combined styrene content of 45wt% was pulverized in advance, with a particle size of 5-15mm, and set aside. Warm up the kneader and set aside.
[0047] Weigh 13.0kg of pulverized SBR, 8.0kg of triphenylmethane triisocyanate, 7.0kg of N-cyclohexyl-N'-phenyl-p-phenylenediamine, and 6.0kg of aluminate coupling agent in a kneader for mixing. Refining, while mixing, add furfural to refine the extracted oil, add in portions, add 5.0kg every 5 minutes, until the added amount reaches 25.0kg, continue to mix, the mixing temperature is 160°C, and refine from 25.0kg of furfural After the extraction oil is completely added, the mixing time is 90 minutes; then extrusion, the extrusion temperature is 140°C. A thick paste is formed after extrusion, resulting in an anti-stripping agent. The distribution ratio of each group is shown in Table 1.
Embodiment 3
[0049] The SBR with a combined styrene content of 34wt% was pulverized in advance, with a particle size of 5-16 mm, and set aside. Warm up the kneader and set aside.
[0050] Weigh 3.2 kg of pulverized SBR, 3.2 kg of triphenylmethane triisocyanate, 3.2 kg of N-phenyl-N'-isopropyl-p-phenylenediamine, and 2.2 kg of silane coupling agent (KH570) and place them in a kneader Carry out mixing inside, add catalytic cracking oil slurry while mixing, add in two times, add 2.4kg every 5 minutes, until the addition amount of catalytic cracking oil slurry reaches 4.8kg, continue mixing, mixing temperature is 135 °C, counting from the time when 4.8kg of catalytic cracking oil slurry is completely added, the mixing time is 65 minutes; then extrude at a temperature of 115 °C to obtain a pasty anti-stripping agent. The distribution ratio of each group is shown in Table 1.
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