CoCrNiAlY multilayer high-temperature protective coating as well as weight gain control method and preparation method thereof
A protective coating and high-temperature technology, applied in coatings, metal material coating technology, high-efficiency propulsion technology, etc., can solve problems such as linear weight gain, achieve the effects of prolonging service life and improving high-temperature oxidation resistance
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Embodiment 1
[0027] The base material is superalloy GH4169, the size of the sample is 15mm×15mm×5mm, and the size of the coating surface (coating area) is 15mm×15mm. Before coating, the surface of the sample is ground, cleaned, sandblasted, and then ultrasonically cleaned; then the treated sample substrate is placed on the turntable in the vacuum chamber of the arc ion plating equipment, and the vacuum is started. up to 6×10 -3 When Pa, argon gas was introduced into the vacuum chamber, and the air pressure was controlled at 0.6Pa; the negative pulse bias voltage of the substrate was controlled to be -120V, and the gas glow discharge was enhanced by the arc, and the surface of the substrate was cleaned by glow discharge ions for 60 minutes; Then start to deposit CoCrNiAlY-Al multi-layer coating (first adjust the Ar gas flow, control the air pressure in the vacuum chamber to 1.2Pa; control the substrate with pulse negative bias to -80V, turn on the CoCrNiAlY target and the Al target at the s...
Embodiment 2
[0029] The base material is titanium alloy (grade Ti6Al4V), the size of the sample is 20mm×20mm×5mm, and the size of the coating surface (coating area) is 20mm×20mm. Before coating, the surface of the sample is polished, cleaned, sandblasted, and then ultrasonically cleaned; then the treated sample substrate is placed on the turntable in the vacuum chamber of the arc ion plating equipment, and the vacuum is started. When the vacuum degree in the vacuum chamber reaches 5.6×10 -3At Pa, argon gas was introduced into the vacuum chamber, and the air pressure was controlled to 0.8Pa; the negative pulse bias voltage of the substrate was controlled to -160V, and the sample was cleaned by glow discharge ions for 60 minutes by arc-enhanced gas glow discharge; then deposition began. CoCrNiAlY-Al multi-layer coating (firstly adjust the Ar gas flow, control the air pressure in the vacuum chamber to 1.1Pa; the substrate plus pulse negative bias is adjusted to -100V, and the CoCrNiAlY target...
Embodiment 3
[0031] The base material is stainless steel (grade 1Cr18Ni9Ti), the size of the sample is 20mm×10mm×10mm, and the size of the coating surface (coating area) is 20mm×10mm. Before coating, the surface of the sample is polished, cleaned, sandblasted, and then ultrasonically cleaned; then the treated sample substrate is placed on the turntable in the vacuum chamber of the arc ion plating equipment, and vacuum is started. When the vacuum degree in the vacuum chamber reaches 4.6×10 -3 At Pa, argon gas was introduced into the vacuum chamber, and the air pressure was controlled at 0.4Pa; the substrate was subjected to a pulsed negative bias voltage of -180V, and the gas glow discharge was enhanced by the arc, and the sample was cleaned by glow discharge ions for 55 minutes; then the deposition started. CoCrNiAlY-Al multi-layer coating (firstly adjust the Ar gas flow, control the air pressure in the vacuum chamber to 1.0Pa; add pulse negative bias to the substrate to -70V, turn on the ...
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