Edible active food fresh-keeping pad and preparation method thereof
A food preservation and activity technology, applied in the direction of climate sustainability, sustainable manufacturing/processing, sustainable packaging industry, etc., can solve the problems of difficult to degrade the polluted environment, unsatisfactory preservation effect of fresh-keeping pads, etc., to achieve rich sources of raw materials, Inhibition of breeding and reproduction, the effect of safe source of raw materials
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Embodiment 1
[0033] An edible active food fresh-keeping pad is prepared according to the following steps:
[0034] Preparation of S1 deacetylated nanochitin:
[0035] Disperse the chitin powder in an aqueous sodium hydroxide solution with a mass volume concentration of 33%, add sodium borohydride accounting for 0.3% of the mass of the chitin powder, and magnetically stir it in a water bath at 90 ° C for 4 hours to obtain deacetylated chitin solution. After suction filtration and washing, the obtained solid product (deionized water was used to wash the solid product several times in the suction filtration process until the washed filtrate was colorless), and then dried in an oven at 45°C for 1 hour. Redissolved in acetic acid aqueous solution with a volume concentration of 1%, ultrasonically treated for 1 h, allowed to stand for 0.5 h, and the supernatant was collected and freeze-dried to obtain deacetylated nanochitin;
[0036] Preparation of S2 carboxymethyl nanocellulose:
[0037] Car...
Embodiment 2
[0044] An edible active food fresh-keeping pad is prepared according to the following steps:
[0045] Preparation of S1 deacetylated nanochitin:
[0046] Disperse the chitin powder in a sodium hydroxide aqueous solution with a mass concentration of 33%, add sodium borohydride accounting for 0.3% of the mass of the chitin powder, and magnetically stir it in a water bath at 90 ° C for 4 hours to obtain a deacetylated chitin solution. . After suction filtration and washing, the obtained solid product (deionized water was used to wash the solid product several times in the suction filtration process until the washed filtrate was colorless), and then dried in an oven at 45°C for 1 hour. Redissolved in acetic acid aqueous solution with a volume concentration of 1%, ultrasonically treated for 1 h, allowed to stand for 0.5 h, and the supernatant was collected and freeze-dried to obtain deacetylated nanochitin;
[0047] Preparation of S2 carboxymethyl nanocellulose:
[0048] Carboxy...
Embodiment 3
[0055] An edible active food fresh-keeping pad is prepared according to the following steps:
[0056] Preparation of S1 deacetylated nanochitin:
[0057] Disperse the chitin powder in an aqueous sodium hydroxide solution with a mass volume concentration of 33%, add sodium borohydride accounting for 0.3% of the mass of the chitin powder, and magnetically stir it in a water bath at 90 ° C for 4 hours to obtain deacetylated chitin solution. After suction filtration and washing, the obtained solid product (deionized water was used to wash the solid product several times in the suction filtration process until the washed filtrate was colorless), and then dried in an oven at 45°C for 1 hour. Redissolved in acetic acid aqueous solution with a volume concentration of 1%, ultrasonically treated for 1 h, allowed to stand for 0.5 h, and the supernatant was collected and freeze-dried to obtain deacetylated nanochitin;
[0058] Preparation of S2 carboxymethyl nanocellulose:
[0059] Car...
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