Application of 1-O-gallic acid acyl-beta-D-glucoside extracted from emblic leafflower fruit in plant disease control
A technology for plant disease control, gallic acid acyl group, applied in the application, sugar derivatives, sugar derivatives, etc., can solve problems such as side effects, environmental and human health threats, reduction of potato tubers, etc.
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Embodiment 1
[0031] A method for preparing 1-O-galloacyl-β-D-glucoside from Emblica, comprising the following steps:
[0032] Step 1. Take 740g of fresh fruit of Amaryllis emblica, remove the core and squeeze the juice to obtain 234g of pomace. The pomace of Amla pomace was placed in a 5000mL beaker, soaked in 2000mL 70% ethanol and leached with ultrasonic acceleration for 1h, repeated the leaching 3 times, combined the extracts, and drained the solvent with a rotary evaporator to obtain a crude extract of the ethanol layer ( EA) 19.74 g.
[0033]Step 2. Take 19.74 g of the crude extract (EA) of the ethanol layer obtained in step 1, dissolve it in 50 mL of 50% methanol water, and use a medium and low pressure reverse phase C18 column (filler: YMC-GEL ODS-A-HG, s-50 μm ; column length is 4.5 × 35 cm), the flow rate is set to 30 mL / min, eluted with 25% methanol aqueous solution, and the 15-31 min fraction (EA-1) is collected.
[0034] Step 3. Dissolve 1.03 g of (EA-1) obtained in step 2 wi...
Embodiment 2
[0050] In the ultra-clean workbench, take the strain (Streptomyces scabies AMCC400023) preserved in the slanted medium, carefully pick a single colony from the inoculated ring after burning and cooling next to the flame of the alcohol lamp, and use the method of streaking on the plate to remove the pathogenic bacteria. Bacteria were inoculated in Gao's No. 1 solid medium, sealed with parafilm, and cultured for 48 h in a constant temperature biochemical incubator at 30 °C. Among them, Gao's No. 1 solid medium (g / L): potassium nitrate: 1.0; potassium dihydrogen phosphate: 0.5; magnesium sulfate: 0.5; ferrous sulfate: 0.01; sodium chloride: 0.5; soluble starch: 20.0; agar : 15.0.
[0051] Pick the activated single colony of Streptomyces scabtus with an inoculation loop, put it on Gao's No. 1 medium, and keep it at a constant temperature of 28 °C for 3 days; suck 3 mL of sterile water on the plate, gently with a blade Scrape off the surface spores, rinse the medium surface spores...
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