Preparation method of gearbox nano-diamond machine olein
A technology of nano-diamond and gearbox, applied in the field of gearbox lubricating oil
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Embodiment 1
[0015] The present invention is a kind of preparation method of gearbox nano-diamond oil, comprising the following steps:
[0016] (1) Nano-diamond is prepared by explosive detonation method, the method is:
[0017] Mix high-energy carbon-rich explosives TNT and RDX in a weight ratio of 50:50, and press them into a cylinder with a cross-sectional diameter of 50mm and a height of 200mm-300mm. The cylinder is hoisted into the detonation kettle, evacuated, and vacuumed. The temperature is -150Pa~-180Pa; then the carbon dioxide gas is injected into the detonation kettle, the pressure value reaches 100KPa~120KPa, the detonation kettle is sealed, and the nano-diamond is synthesized by detonating with a detonator;
[0018] (2) Chemical treatment of nano-diamonds to remove organic matter and impurities and improve the purity of nano-diamonds by:
[0019] Take 1kg of nano-diamonds made by detonation method, put it into a container, add 20L of hydrochloric acid with a volume concentrat...
Embodiment 2
[0030] The present invention is a kind of preparation method of gearbox nano-diamond oil, comprising the following steps:
[0031] (1) Nano-diamond is prepared by explosive detonation method, the method is:
[0032] The high-energy carbon-rich explosive TNT and RDX are mixed together in a weight ratio of 50:50, and pressed into a cylinder with a cross-sectional diameter of 50mm and a height of 250mm. -160Pa; then pour carbon dioxide gas into the detonation kettle, the pressure value reaches 110KPa, seal the detonation kettle, and use a detonator to detonate to synthesize nanodiamonds;
[0033] (2) Chemical treatment of nano-diamonds to remove organic matter and impurities and improve the purity of nano-diamonds by:
[0034] Take 1kg of nano-diamonds made by detonation method, put it into a container, add 20L of hydrochloric acid with a volume concentration of 35%, stir evenly, heat, continue to boil for 1 hour after boiling, rinse with distilled water until neutral, and remov...
Embodiment 3
[0045] The present invention is a kind of preparation method of gearbox nano-diamond oil, comprising the following steps:
[0046] (1) Nano-diamond is prepared by explosive detonation method, the method is:
[0047] The high-energy carbon-rich explosive TNT and RDX are mixed together in a weight ratio of 50:50, and pressed into a cylinder with a cross-sectional diameter of 50mm and a height of 200mm. -175Pa; then pour carbon dioxide gas into the detonation kettle, the pressure value reaches 100KPa, seal the detonation kettle, and use a detonator to detonate to synthesize nanodiamonds;
[0048] (2) Chemical treatment of nano-diamonds to remove organic matter and impurities and improve the purity of nano-diamonds by:
[0049] Take 1kg of nano-diamonds made by detonation method, put it into a container, add 20L of hydrochloric acid with a volume concentration of 35%, stir evenly, heat, continue to boil for 1 hour after boiling, rinse with distilled water until neutral, and remov...
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