Preparation method of polyester fabric moisture absorption and sweat releasing finishing agent containing naphthalene structure
A technology for moisture-absorbing and sweat-wicking polyester fabrics is applied in the field of preparation of moisture-absorbing and sweat-wicking finishing agents, which can solve the problems of difficulty in washing and removing stains, limitations, and long process time, so as to reduce carbon and sewage emissions, and save water and energy. , the effect of reducing the process time
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Embodiment 1
[0016] Synthesis of the moisture-absorbing and perspiring agent containing naphthalene structure: First, 70 g of polyethylene glycol was dehydrated, and the temperature was controlled at 100-105 °C for vacuum dehydration for 1 hour. After the dehydration is completed, 15g of dimethyl 1,8-naphthalenedicarboxylate, 15g of ethylene glycol, and 0.03g of zinc acetate are successively added to the reaction vessel equipped with a thermometer and a nitrogen tube, and the temperature is slowly raised under nitrogen protection for 25 to 30 minutes. When the temperature rose to 170°C, the temperature was controlled at 170-180°C for 4 hours.
[0017] After the transesterification is completed, continue to heat up to 190°C, control the temperature at 190-200°C and react for 30min, start vacuuming, and continue to heat up to 230°C, control the temperature at 220-230°C, and wait until the vacuum degree in the reaction vessel reaches -0.099MPa or more Timely heat preservation for 3 hours, and...
Embodiment 2
[0019] Synthesis of the moisture-absorbing and perspiring agent containing naphthalene structure: First, 65 g of polyethylene glycol was dehydrated, and the temperature was controlled at 100-105 °C for vacuum dehydration for 1 hour. After the dehydration was completed, 20g of dimethyl 1,8-naphthalene dicarboxylate, 15g of ethylene glycol, 0.03g of magnesium acetate were successively added to the reaction vessel equipped with a thermometer and a nitrogen tube, and the temperature was slowly raised under nitrogen protection for 25-30 minutes. When the temperature rose to 170°C, the temperature was controlled at 170-180°C for 4 hours.
[0020] After the transesterification is completed, continue to heat up to 190°C, control the temperature at 190-200°C and react for 30min, start vacuuming, and continue to heat up to 230°C, control the temperature at 220-230°C, and wait until the vacuum degree in the reaction vessel reaches -0.099MPa or more Timely heat preservation for 3 hours, a...
Embodiment 3
[0022] Synthesis of a moisture-absorbing and perspiring agent containing a naphthalene structure: firstly, 60 g of polyethylene glycol was subjected to dehydration treatment, and the temperature was controlled at 100-105 °C for vacuum dehydration for 1 hour. After the dehydration is completed, 25g of dimethyl 1,8-naphthalenedicarboxylate, 15g of ethylene glycol, 0.03g of calcium acetate are added successively to the reaction vessel equipped with a thermometer and a nitrogen tube, and the temperature is slowly raised under nitrogen protection for 25-30 minutes. When the temperature rose to 170°C, the temperature was controlled at 170-180°C for 4 hours.
[0023] After the transesterification is completed, continue to heat up to 190 °C, control the temperature at 190 to 200 °C for 30 minutes, start vacuuming, and continue to heat up to 230 °C, control the temperature at 220 to 230 °C, and wait until the vacuum degree in the reaction vessel reaches -0.099MPa or more Timely heat pr...
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